Technology Process of C16H11(2)HO
There total 3 articles about C16H11(2)HO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / methanol; toluene / 24 h / Reflux
2: boron tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere
3: water-d2 / acetonitrile / 1 h / Inert atmosphere; UV-irradiation
With
tetrakis(triphenylphosphine) palladium(0); water-d2; boron tribromide; potassium carbonate;
In
methanol; dichloromethane; toluene; acetonitrile;
1: |Suzuki Coupling;
DOI:10.1021/jo301456y
- Guidance literature:
-
With
water-d2;
In
acetonitrile;
for 1h;
Inert atmosphere;
UV-irradiation;
DOI:10.1021/jo301456y
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / methanol; toluene / 24 h / Reflux
2: boron tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere
3: water-d2 / acetonitrile / 1 h / Inert atmosphere; UV-irradiation
With
tetrakis(triphenylphosphine) palladium(0); water-d2; boron tribromide; potassium carbonate;
In
methanol; dichloromethane; toluene; acetonitrile;
1: |Suzuki Coupling;
DOI:10.1021/jo301456y