C₆₆H₈₀O₁₀Si

Base Information

• Chemical Name: C₆₆H₈₀O₁₀Si
• CAS No.: 1225283-75-9
• Molecular Formula: C₆₆H₈₀O₁₀Si
• Molecular Weight: 1061.44
• Mol file: 1225283-75-9.mol

Synonyms:

Chemical Property of C₆₆H₈₀O₁₀Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₆H₈₀O₁₀Si

There total 8 articles about C₆₆H₈₀O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(11-silylundecyloxy)benzoic acid (1225283-63-5) + C45H46O8 (1225283-71-5) → C66H80O10Si (1225283-75-9)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In chloroform; at 20 ℃;

DOI:10.1021/cm100134f

Reference yield:

C52H52O8 → C66H80O10Si (1225283-75-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 20 °C

2: dmap; dicyclohexyl-carbodiimide / chloroform / 20 °C

With dmap; 20 % Pd(OH)2/C; hydrogen; dicyclohexyl-carbodiimide; In chloroform; ethyl acetate;

DOI:10.1021/cm100134f

Reference yield:

3-Bromophenol (591-20-8) → C66H80O10Si (1225283-75-9)

Guidance literature:

Multi-step reaction with 6 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 15 h / Reflux

2: dmap; dicyclohexyl-carbodiimide / chloroform / 20 °C

3: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 20 °C

4: dmap; dicyclohexyl-carbodiimide / chloroform / 20 °C

5: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 20 °C

6: dmap; dicyclohexyl-carbodiimide / chloroform / 20 °C

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 20 % Pd(OH)2/C; hydrogen; sodium carbonate; dicyclohexyl-carbodiimide; In 1,2-dimethoxyethane; chloroform; water; ethyl acetate;

DOI:10.1021/cm100134f

upstream raw materials:

4-(11-silylundecyloxy)benzoic acid

C₄₅H₄₆O₈

3-Bromophenol

[4-(benzyloxy)phenyl]boronic acid