C₅₄H₅₄N₂O₇Si₂

Base Information

• Chemical Name: C₅₄H₅₄N₂O₇Si₂
• CAS No.: 1352916-65-4
• Molecular Formula: C₅₄H₅₄N₂O₇Si₂
• Molecular Weight: 899.203
• Mol file: 1352916-65-4.mol

Synonyms:

Chemical Property of C₅₄H₅₄N₂O₇Si₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₅₄H₅₄N₂O₇Si₂

There total 1 articles about C₅₄H₅₄N₂O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

FL-120B + tert-butylchlorodiphenylsilane (58479-61-1) → C54H54N2O7Si2 (1352916-65-4)

Guidance literature:

With 1H-imidazole; dmap; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1002/anie.201104504

Reference yield:

C54H54N2O7Si2 (1352916-65-4) → C50H48N2O6Si2 (1352916-67-6)

Guidance literature:

With dihydrogen peroxide; lithium hydroxide; In tetrahydrofuran; water; at 0 ℃; for 96h; Inert atmosphere;

DOI:10.1002/anie.201104504

Reference yield:

C54H54N2O7Si2 (1352916-65-4) → C52H50N2O7Si2 (1352916-64-3)

Guidance literature:

Multi-step reaction with 2 steps

1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 96 h / 0 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With dmap; dihydrogen peroxide; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; water;

DOI:10.1002/anie.201104504

upstream raw materials:

tert-butylchlorodiphenylsilane

Downstream raw materials:

C₅₂H₅₀N₂O₇Si₂

FL-120B'

C₅₀H₄₈N₂O₆Si₂