trans-2-<<2-(1H-indol-3-yl)ethyl>amino>-trans-5-phenoxycyclopentanol

Base Information

Chemical Name:trans-2-<<2-(1H-indol-3-yl)ethyl>amino>-trans-5-phenoxycyclopentanol
CAS No.:97072-04-3
Molecular Formula:C₂₁H₂₄N₂O₂
Molecular Weight:336.434
Hs Code.:

Synonyms:

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Chemical Property of trans-2-<<2-(1H-indol-3-yl)ethyl>amino>-trans-5-phenoxycyclopentanol

Chemical Property:

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Technology Process of trans-2-<<2-(1H-indol-3-yl)ethyl>amino>-trans-5-phenoxycyclopentanol

There total 6 articles about trans-2-<<2-(1H-indol-3-yl)ethyl>amino>-trans-5-phenoxycyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3212-60-0,6426-28-4,62894-08-0,109431-72-3
cyclopent-2-enol

: 97072-04-3
trans-2-<<2-(1H-indol-3-yl)ethyl>amino>-trans-5-phenoxycyclopentanol

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / vanadyl acetylacetonate, tert-butyl hydroperoxide / benzene / 1.) 80 deg C, 15 min, 2.) 40 deg C, 5 h

2: 79.5 percent / triphenylphosphine, isopropyl azocarboxylate / tetrahydrofuran / 24 h / Ambient temperature

3: 4.3 g / ethanol / 24 h / Heating

With tert.-butylhydroperoxide; di-isopropyl azodicarboxylate; vanadyl acetylacetonate; triphenylphosphine; In tetrahydrofuran; ethanol; benzene;
DOI:10.1021/jo00217a017

Reference yield:

: 95526-36-6
1-phenoxy-2-cyclopentene

: 97072-04-3
trans-2-<<2-(1H-indol-3-yl)ethyl>amino>-trans-5-phenoxycyclopentanol

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / 3-chloroperbenzoic acid (MCBA) / CH₂Cl₂ / 15 h / 4 - 20 °C

2: 4.3 g / ethanol / 24 h / Heating

With 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane;
DOI:10.1021/jo00217a017

Reference yield:

: 25484-62-2,29782-88-5,765-54-8,25516-47-6,34310-95-7,120577-03-9,139015-06-8
cis-6-oxabicyclo<3.1.0>cyclohexan-2-ol

: 97072-04-3
trans-2-<<2-(1H-indol-3-yl)ethyl>amino>-trans-5-phenoxycyclopentanol

Guidance literature:: Multi-step reaction with 2 steps

1: 79.5 percent / triphenylphosphine, isopropyl azocarboxylate / tetrahydrofuran / 24 h / Ambient temperature

2: 4.3 g / ethanol / 24 h / Heating

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; ethanol;
DOI:10.1021/jo00217a017