4-(N-methyl)benzamido-3-tert-butyl-3aα,5,6,6aα-tetrahydro-4βH-cyclopentisoxazole

Base Information

Chemical Name:4-(N-methyl)benzamido-3-tert-butyl-3aα,5,6,6aα-tetrahydro-4βH-cyclopentisoxazole
CAS No.:127311-23-3
Molecular Formula:C₁₈H₂₄N₂O₂
Molecular Weight:300.401
Hs Code.:

4-(N-methyl)benzamido-3-tert-butyl-3aα,5,6,6aα-tetrahydro-4βH-cyclopent<d>isoxazole

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(N-methyl)benzamido-3-tert-butyl-3aα,5,6,6aα-tetrahydro-4βH-cyclopentisoxazole

Chemical Property:

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Technology Process of 4-(N-methyl)benzamido-3-tert-butyl-3aα,5,6,6aα-tetrahydro-4βH-cyclopentisoxazole

There total 5 articles about 4-(N-methyl)benzamido-3-tert-butyl-3aα,5,6,6aα-tetrahydro-4βH-cyclopentisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3273-26-5
1-chloro-2,2-dimethyl-propan-1-one oxime

: 127310-74-1
N-(cyclopent-2-en-1-yl)-N-methylbenzamide

: 127311-23-3
4-(N-methyl)benzamido-3-tert-butyl-3aα,5,6,6aα-tetrahydro-4βH-cyclopentisoxazole

: 127311-22-2,127380-40-9
6-(N-methyl)benzamido-3-tert-butyl-3aα,5,6β,6aα-tetrahydro-4H-cyclopentisoxazole

: 127311-22-2,127380-40-9
6-(N-methyl)benzamido-3-tert-butyl-3aα,5,6α,6aα-tetrahydro-4H-cyclopentisoxazole

Guidance literature:: With triethylamine; In benzene; at 80 - 84 ℃; for 228h; Yield given. Yields of byproduct given;

Reference yield:

: 3350-06-9
2-cyclopentenamine

: 127311-23-3
4-(N-methyl)benzamido-3-tert-butyl-3aα,5,6,6aα-tetrahydro-4βH-cyclopentisoxazole

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / aq. NaOH / 0.5 h / 25 °C

2: Et₃N / benzene / 108 h / 25 °C

3: 1.) NaH / 1.) THF, 25 deg C, 1 h, 2.) THF, 25 deg C, 5 h

With sodium hydroxide; sodium hydride; triethylamine; In benzene;

Reference yield:

: 3551-51-7
N-(cyclopent-2-en-1-yl)-benzamide

: 127311-23-3
4-(N-methyl)benzamido-3-tert-butyl-3aα,5,6,6aα-tetrahydro-4βH-cyclopentisoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / benzene / 108 h / 25 °C

2: 1.) NaH / 1.) THF, 25 deg C, 1 h, 2.) THF, 25 deg C, 5 h

With sodium hydride; triethylamine; In benzene;