C₂₆H₄₂O₈

Base Information

Chemical Name:C₂₆H₄₂O₈
CAS No.:1360872-89-4
Molecular Formula:C₂₆H₄₂O₈
Molecular Weight:482.615
Hs Code.:

C<sub>26</sub>H<sub>42</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C₂₆H₄₂O₈

Chemical Property:

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Technology Process of C₂₆H₄₂O₈

There total 25 articles about C₂₆H₄₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₅H₆₂O₈Si

: 1360872-89-4
C₂₆H₄₂O₈

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1002/chem.201101437

Reference yield:

: 908865-92-9
(2S,3S)-6-(tert-Butyl-diphenyl-silanyloxy)-3-(4-methoxy-benzyloxy)-2-methyl-hexan-1-ol

: 1360872-89-4
C₂₆H₄₂O₈

Guidance literature:: Multi-step reaction with 16 steps

1.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.75 h / 20 °C

2.1: tert.-butyl lithium; 9-methoxy-9-BBN / tetrahydrofuran; diethyl ether; hexane; pentane / 1.17 h / -78 - 20 °C

2.2: 50 °C

3.1: 2,3-Dimethyl-2-butene; dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

3.2: 0 - 20 °C

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 °C / pH 7 / aq. phosphate buffer

6.1: zinc trifluoromethanesulfonate / dichloromethane / 12 h / 20 °C

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / -78 °C

7.2: -78 - 0 °C

8.1: 20% palladium hydroxide on charcoal; hydrogen / ethyl acetate / 20 °C

9.1: 1H-imidazole / dichloromethane / 7.5 h / 20 °C

10.1: 2,6-dimethylpyridine / dichloromethane / 1.67 h / -78 °C

11.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1.5 h / -78 - 20 °C

12.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 9 h / 20 °C

13.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 0 - 115 °C / Microwave irradiation

14.1: potassium hydroxide / tetrahydrofuran; methanol / 9.5 h / 70 °C

15.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

16.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; osmium(VIII) oxide; tetrapropylammonium perruthennate; 2,3-Dimethyl-2-butene; dimethylsulfide borane complex; 20% palladium hydroxide on charcoal; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; iodine; tert.-butyl lithium; zinc trifluoromethanesulfonate; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 9-methoxy-9-BBN; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; tert-butyl alcohol; pentane; 2.2: Suzuki-Miyaura coupling;
DOI:10.1002/chem.201101437

Reference yield:

: 1028432-61-2
C₅₂H₆₄O₆Si

: 1360872-89-4
C₂₆H₄₂O₈

Guidance literature:: Multi-step reaction with 14 steps

1.1: 2,3-Dimethyl-2-butene; dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 °C / pH 7 / aq. phosphate buffer

4.1: zinc trifluoromethanesulfonate / dichloromethane / 12 h / 20 °C

5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / -78 °C

5.2: -78 - 0 °C

6.1: 20% palladium hydroxide on charcoal; hydrogen / ethyl acetate / 20 °C

7.1: 1H-imidazole / dichloromethane / 7.5 h / 20 °C

8.1: 2,6-dimethylpyridine / dichloromethane / 1.67 h / -78 °C

9.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1.5 h / -78 - 20 °C

10.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 9 h / 20 °C

11.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 0 - 115 °C / Microwave irradiation

12.1: potassium hydroxide / tetrahydrofuran; methanol / 9.5 h / 70 °C

13.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

14.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; osmium(VIII) oxide; tetrapropylammonium perruthennate; 2,3-Dimethyl-2-butene; dimethylsulfide borane complex; 20% palladium hydroxide on charcoal; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; zinc trifluoromethanesulfonate; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; tert-butyl alcohol;
DOI:10.1002/chem.201101437