C₃₃H₃₂N₂O₈

Base Information

Chemical Name:C₃₃H₃₂N₂O₈
CAS No.:1239442-66-0
Molecular Formula:C₃₃H₃₂N₂O₈
Molecular Weight:584.626
Hs Code.:

C<sub>33</sub>H<sub>32</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₃₂N₂O₈

Chemical Property:

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Technology Process of C₃₃H₃₂N₂O₈

There total 5 articles about C₃₃H₃₂N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 334002-79-8
lithium 4-isopropylphenoxide

: 83928-84-1
7-cyano-7-(ethoxycarbonyl)-1,4-benzoquinonemethide

: 1239442-61-5
C₂₂H₂₃NO₅

: 1239442-62-6
C₂₂H₂₃NO₅

: 1239442-65-9
C₃₃H₃₂N₂O₈

: 1239442-66-0
C₃₃H₃₂N₂O₈

: 1239442-64-8
C₃₃H₃₂N₂O₈

: 1239442-63-7
C₃₃H₃₂N₂O₈

Guidance literature:: With (-)-sparteine; In dichloromethane; toluene; at -78 ℃; for 12h; optical yield given as %ee; stereoselective reaction;
DOI:10.1021/ma100866n

Reference yield:

: 334002-79-8
lithium 4-isopropylphenoxide

: 83928-84-1
7-cyano-7-(ethoxycarbonyl)-1,4-benzoquinonemethide

: 1239442-65-9
C₃₃H₃₂N₂O₈

: 1239442-66-0
C₃₃H₃₂N₂O₈

: 1239442-64-8
C₃₃H₃₂N₂O₈

: 1239442-63-7
C₃₃H₃₂N₂O₈

Guidance literature:: lithium 4-isopropylphenoxide; With (S,S)-2,2'-isopropylidenebis(4-phenyl-2-oxazoline); In dichloromethane; toluene; at -78 ℃; for 12h; Inert atmosphere;

7-cyano-7-(ethoxycarbonyl)-1,4-benzoquinonemethide; In dichloromethane; toluene; at -78 ℃; Inert atmosphere;

With acetic acid; In dichloromethane; toluene; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1002/pola.25054

Reference yield:

: 83928-82-9
4-[1'-cyano-1'-(ethoxycarbonyl)methylene]cyclohexanone

: 1239442-65-9
C₃₃H₃₂N₂O₈

: 1239442-66-0
C₃₃H₃₂N₂O₈

: 1239442-64-8
C₃₃H₃₂N₂O₈

: 1239442-63-7
C₃₃H₃₂N₂O₈

Guidance literature:: Multi-step reaction with 2 steps

1.1: manganese(IV) oxide / chloroform / Molecular sieve; Reflux

2.1: (S,S)-2,2'-isopropylidenebis(4-phenyl-2-oxazoline) / dichloromethane; toluene / 12 h / -78 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

2.3: Inert atmosphere

With manganese(IV) oxide; (S,S)-2,2'-isopropylidenebis(4-phenyl-2-oxazoline); In dichloromethane; chloroform; toluene;
DOI:10.1002/pola.25054