C₅₁H₆₀N₂O₁₀

Base Information

Chemical Name:C₅₁H₆₀N₂O₁₀
CAS No.:1314865-20-7
Molecular Formula:C₅₁H₆₀N₂O₁₀
Molecular Weight:861.045
Hs Code.:

C<sub>51</sub>H<sub>60</sub>N<sub>2</sub>O<sub>10</sub>

Synonyms:

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Chemical Property of C₅₁H₆₀N₂O₁₀

Chemical Property:

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Technology Process of C₅₁H₆₀N₂O₁₀

There total 8 articles about C₅₁H₆₀N₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1314865-18-3
2-[(N,N'-benzyl-benzyloxycarbonyl)amino]ethyl O-(4-azido-3-O-benzyl-4,6-dideoxy-2-O-methyl-R-D-glucopyranosyl)-(1→3)-2,4-di-O-benzyl-R-L-rhamnopyranoside

: 1314865-20-7
C₅₁H₆₀N₂O₁₀

Guidance literature:: With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In ethanol; dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jo200340q

Reference yield:

: 2-[(N-benzyloxycarbonyl)amino]ethyl L-rhamnopyranoside

: 1314865-20-7
C₅₁H₆₀N₂O₁₀

Guidance literature:: Multi-step reaction with 7 steps

1.1: di(n-butyl)tin oxide / methanol / 5 h / Reflux

1.2: 5 h

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 0.5 h / 0 °C

4.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / -40 °C / Molecular sieve; Inert atmosphere

5.1: sodium methylate / methanol / 12 h / 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 °C

7.1: sodium tetrahydroborate; nickel(II) chloride hexahydrate / ethanol; dichloromethane / 1 h / 20 °C

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; trimethylsilyl trifluoromethanesulfonate; sodium methylate; sodium hydride; di(n-butyl)tin oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo200340q

Reference yield:

: 1314865-13-8
2-[(N-benzyloxycarbonyl)amino]ethyl 3-O-(3-methoxy)-benzyl-α-L-rhamnopyranoside

: 1314865-20-7
C₅₁H₆₀N₂O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 0.5 h / 0 °C

3: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / -40 °C / Molecular sieve; Inert atmosphere

4: sodium methylate / methanol / 12 h / 20 °C

5: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 °C

6: sodium tetrahydroborate; nickel(II) chloride hexahydrate / ethanol; dichloromethane / 1 h / 20 °C

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; trimethylsilyl trifluoromethanesulfonate; sodium methylate; sodium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo200340q