cis-3-{{2-[2-(4-methylphenyl)ethenyl]phenyl}methyl}sydnone

Base Information

Chemical Name:cis-3-{{2-[2-(4-methylphenyl)ethenyl]phenyl}methyl}sydnone
CAS No.:1370007-93-4
Molecular Formula:C₁₈H₁₆N₂O₂
Molecular Weight:292.337
Hs Code.:

Synonyms:

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Chemical Property of cis-3-{{2-[2-(4-methylphenyl)ethenyl]phenyl}methyl}sydnone

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Technology Process of cis-3-{{2-[2-(4-methylphenyl)ethenyl]phenyl}methyl}sydnone

There total 6 articles about cis-3-{{2-[2-(4-methylphenyl)ethenyl]phenyl}methyl}sydnone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1370007-85-4
C₂₀H₂₃NO₂

: 1370007-93-4
cis-3-{{2-[2-(4-methylphenyl)ethenyl]phenyl}methyl}sydnone

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; sodium hydroxide / 4 h / Reflux

2.1: sodium hydroxide / water / 1 h

2.2: 0.5 h / 20 °C

2.3: 240 h / Darkness

With water; sodium hydroxide; In water;
DOI:10.3762/bjoc.7.196

Reference yield:

: 529-19-1
2-Methylbenzonitrile

: 1370007-93-4
cis-3-{{2-[2-(4-methylphenyl)ethenyl]phenyl}methyl}sydnone

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 1 h / Reflux

2.1: toluene / 20 - 50 °C

3.1: sodium / ethanol / 20 °C / Inert atmosphere

4.1: lithium aluminium tetrahydride / diethyl ether / 20 °C / Reflux

5.1: sodium acetate / ethanol / 1.5 h / Reflux

6.1: water; sodium hydroxide / 4 h / Reflux

7.1: sodium hydroxide / water / 1 h

7.2: 0.5 h / 20 °C

7.3: 240 h / Darkness

With N-Bromosuccinimide; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); water; sodium acetate; sodium; sodium hydroxide; In tetrachloromethane; diethyl ether; ethanol; water; toluene; 3.1: Wittig reaction;
DOI:10.3762/bjoc.7.196

Reference yield:

: 1370007-77-4
2-(bromomethyl)benzonitrile

: 1370007-93-4
cis-3-{{2-[2-(4-methylphenyl)ethenyl]phenyl}methyl}sydnone

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 20 °C / Reflux

2.1: sodium acetate / ethanol / 1.5 h / Reflux

3.1: water; sodium hydroxide / 4 h / Reflux

4.1: sodium hydroxide / water / 1 h

4.2: 0.5 h / 20 °C

4.3: 240 h / Darkness

With lithium aluminium tetrahydride; water; sodium acetate; sodium hydroxide; In diethyl ether; ethanol; water;
DOI:10.3762/bjoc.7.196