iodure de <(diphenyl-4,6 thiopyrannylidene-2) methyl>-3 p-methoxyphenyl-5 dithiole-1,2 ylium

Base Information

Chemical Name:iodure de <(diphenyl-4,6 thiopyrannylidene-2) methyl>-3 p-methoxyphenyl-5 dithiole-1,2 ylium
CAS No.:77643-71-1
Molecular Formula:C₂₈H₂₁OS₃*I
Molecular Weight:596.577
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of iodure de <(diphenyl-4,6 thiopyrannylidene-2) methyl>-3 p-methoxyphenyl-5 dithiole-1,2 ylium

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Technology Process of iodure de <(diphenyl-4,6 thiopyrannylidene-2) methyl>-3 p-methoxyphenyl-5 dithiole-1,2 ylium

There total 2 articles about iodure de <(diphenyl-4,6 thiopyrannylidene-2) methyl>-3 p-methoxyphenyl-5 dithiole-1,2 ylium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1033-40-5
iodure de methylthio-2 diphenyl-4,6 thiopyrylium

: 59704-71-1
3-(4-Methoxy-phenyl)-5-methyl-[1,2]dithiol-1-ylium; iodide

: 77643-71-1
iodure de <(diphenyl-4,6 thiopyrannylidene-2) methyl>-3 p-methoxyphenyl-5 dithiole-1,2 ylium

Guidance literature:: In butan-1-ol; for 4h; Heating;

Reference yield:

: 4023-80-7
1-(4-methoxyphenyl)butan-1,3-dione

: 77643-71-1
iodure de <(diphenyl-4,6 thiopyrannylidene-2) methyl>-3 p-methoxyphenyl-5 dithiole-1,2 ylium

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) P₂S₅ 2.) KI / 1.) xylene, 120 degC, 2h 2.) H₂O

2: 66 percent / butan-1-ol / 4 h / Heating

With tetraphosphorus decasulfide; potassium iodide; In butan-1-ol;

Reference yield:

: 77643-71-1
iodure de <(diphenyl-4,6 thiopyrannylidene-2) methyl>-3 p-methoxyphenyl-5 dithiole-1,2 ylium

: 77643-79-9
(diphenyl-5,7 dithia-1,4 indenylidene-2)-2p-methoxyphenyl-1 ethanone

Guidance literature:: With chlorure de benzohydroxymoyle; triethylamine; Yield given. Multistep reaction; 1. DMF, 20 h 2.) benzene, 0.5 h, reflux;