C₁₂H₁₈NO₁₅P₃

Base Information

Chemical Name:C₁₂H₁₈NO₁₅P₃
CAS No.:1364927-43-4
Molecular Formula:C₁₂H₁₈NO₁₅P₃
Molecular Weight:509.194
Hs Code.:

C<sub>12</sub>H<sub>18</sub>NO<sub>15</sub>P<sub>3</sub>

Synonyms:

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Chemical Property of C₁₂H₁₈NO₁₅P₃

Chemical Property:

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Technology Process of C₁₂H₁₈NO₁₅P₃

There total 10 articles about C₁₂H₁₈NO₁₅P₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1364927-31-0
C₁₂H₁₅NO₆

: 1364927-43-4
C₁₂H₁₈NO₁₅P₃

Guidance literature:: C₁₂H₁₅NO₆; With trimethyl phosphite; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate; at -15 - -10 ℃; Inert atmosphere;

With tributyl-amine; tri-n-butylamine pyrophosphate; In N,N-dimethyl-formamide; at -10 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/chem.201102066

Reference yield:

: 1241725-14-3
C₁₇H₃₆O₃Si₂

: 1364927-43-4
C₁₂H₁₈NO₁₅P₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: tributyl-amine; triphenyl-arsane; palladium diacetate / N,N-dimethyl-formamide / 15 h / 20 - 70 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

3.1: sodium triacetoxyborohydride; acetic acid / acetonitrile / 1 h / 0 °C / Inert atmosphere

4.1: pyridine / 2.15 h / 20 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 1 h / 20 °C / Inert atmosphere

6.1: tert.-butylhydroperoxide; potassium iodide / water; acetonitrile / 2 h / 75 °C / Darkness; Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

8.1: trimethyl phosphite; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate / -15 - -10 °C / Inert atmosphere

8.2: 0.5 h / -10 °C / Inert atmosphere

With pyridine; trimethyl phosphite; tert.-butylhydroperoxide; tributyl-amine; triphenyl-arsane; palladium 10% on activated carbon; sodium triacetoxyborohydride; tetrabutyl ammonium fluoride; hydrogen; palladium diacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; acetic acid; triethylamine; potassium iodide; trichlorophosphate; In tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 1.1: Heck reaction;
DOI:10.1002/chem.201102066

Reference yield:

: C₂₁H₂₅NO₆

: 1364927-43-4
C₁₂H₁₈NO₁₅P₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / 2.15 h / 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 1 h / 20 °C / Inert atmosphere

3.1: tert.-butylhydroperoxide; potassium iodide / water; acetonitrile / 2 h / 75 °C / Darkness; Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

5.1: trimethyl phosphite; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate / -15 - -10 °C / Inert atmosphere

5.2: 0.5 h / -10 °C / Inert atmosphere

With pyridine; trimethyl phosphite; tert.-butylhydroperoxide; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; triethylamine; potassium iodide; trichlorophosphate; In tetrahydrofuran; water; ethyl acetate; acetonitrile;
DOI:10.1002/chem.201102066