N-phenylhexanoimidoyl chloride

Base Information

• Chemical Name: N-phenylhexanoimidoyl chloride
• CAS No.: 1355576-08-7
• Molecular Formula: C₁₂H₁₆ClN
• Molecular Weight: 209.719
• Mol file: 1355576-08-7.mol

Synonyms:

Chemical Property of N-phenylhexanoimidoyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-phenylhexanoimidoyl chloride

There total 3 articles about N-phenylhexanoimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(n-hexanoyl)aniline (621-15-8) → N-phenylhexanoimidoyl chloride (1355576-08-7)

Guidance literature:

With 2,6-dimethylpyridine; oxalyl dichloride; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1021/jm201463v

Reference yield:

aniline (62-53-3) → N-phenylhexanoimidoyl chloride (1355576-08-7)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / ethyl acetate / 20 °C

2: 2,6-dimethylpyridine; oxalyl dichloride / dichloromethane / 0.5 h / 0 °C

With 2,6-dimethylpyridine; oxalyl dichloride; triethylamine; In dichloromethane; ethyl acetate;

DOI:10.1021/jm201463v

Reference yield:

n-valeryl chloride (638-29-9) → N-phenylhexanoimidoyl chloride (1355576-08-7)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / ethyl acetate / 20 °C

2: 2,6-dimethylpyridine; oxalyl dichloride / dichloromethane / 0.5 h / 0 °C

With 2,6-dimethylpyridine; oxalyl dichloride; triethylamine; In dichloromethane; ethyl acetate;

DOI:10.1021/jm201463v

upstream raw materials:

N-(n-hexanoyl)aniline

n-valeryl chloride

aniline

Downstream raw materials:

3-(N-phenylhexanoimidoyl)-1-(3-pyridylmethyl)thiourea