1,1-dimethylethyl amino>-2,3-O-(1-methyl-ethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

Base Information

Chemical Name:1,1-dimethylethyl amino>-2,3-O-(1-methyl-ethylidene)-β-D-ribo-dec-5-enofuranosid>uronates
CAS No.:124288-77-3
Molecular Formula:C₂₅H₃₆N₂O₁₀S
Molecular Weight:556.634
Hs Code.:

1,1-dimethylethyl <methyl-6-nitro-5,6,7,8,9,-pentadeoxy-9(S)-<<(4-methylphenyl)sulfonyl>amino>-2,3-O-(1-methyl-ethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

Synonyms:

Suppliers and Price of 1,1-dimethylethyl amino>-2,3-O-(1-methyl-ethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,1-dimethylethyl amino>-2,3-O-(1-methyl-ethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,1-dimethylethyl amino>-2,3-O-(1-methyl-ethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

There total 6 articles about 1,1-dimethylethyl amino>-2,3-O-(1-methyl-ethylidene)-β-D-ribo-dec-5-enofuranosid>uronates which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 124288-76-2
(S)-6-Hydroxy-6-((3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-5-nitro-2-(toluene-4-sulfonylamino)-hexanoic acid tert-butyl ester

: 124288-77-3,124288-96-6
1,1-dimethylethyl amino>-2,3-O-(1-methyl-ethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

Guidance literature:: With dicyclohexyl-carbodiimide; copper(l) chloride; In acetonitrile; at 35 ℃; for 16h;
DOI:10.1021/jo00290a028

Reference yield:

: 124288-73-9
1,1-dimethylethyl (S)-2-<<(4-methylphenyl)sulfonyl>-amino>-5-<<(phenylmethoxy)carbonyl>amino>pentanoate

: 124288-77-3,124288-96-6
1,1-dimethylethyl amino>-2,3-O-(1-methyl-ethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / H₂ / 10percent Pd/C / methanol / 3102.9 Torr

2: 56 percent / m-CPBA / CH₂Cl₂ / 0.28 h / Heating

3: 86 percent / KF / acetonitrile / 24 h / 22 °C

4: 96 percent / dicyclohexylcarbodiimde, copper(I) chloride / acetonitrile / 16 h / 35 °C

With potassium fluoride; hydrogen; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; copper(l) chloride; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo00290a028

Reference yield:

: 110414-90-9
α-N-tosyl-δ-N-carbobenzoxyornthine

: 124288-77-3,124288-96-6
1,1-dimethylethyl amino>-2,3-O-(1-methyl-ethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / CHCl₃ / 22 h / 22 °C

2: 99 percent / H₂ / 10percent Pd/C / methanol / 3102.9 Torr

3: 56 percent / m-CPBA / CH₂Cl₂ / 0.28 h / Heating

4: 86 percent / KF / acetonitrile / 24 h / 22 °C

5: 96 percent / dicyclohexylcarbodiimde, copper(I) chloride / acetonitrile / 16 h / 35 °C

With potassium fluoride; hydrogen; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; copper(l) chloride; palladium on activated charcoal; In methanol; dichloromethane; chloroform; acetonitrile;
DOI:10.1021/jo00290a028