bis(2-ethylhexyl) 2,5-diiodoterephthalate

Base Information

• Chemical Name: bis(2-ethylhexyl) 2,5-diiodoterephthalate
• CAS No.: 935271-96-8
• Molecular Formula: C₂₄H₃₆I₂O₄
• Molecular Weight: 642.356
• Mol file: 935271-96-8.mol

Synonyms:

Chemical Property of bis(2-ethylhexyl) 2,5-diiodoterephthalate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(2-ethylhexyl) 2,5-diiodoterephthalate

There total 2 articles about bis(2-ethylhexyl) 2,5-diiodoterephthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

2-Ethylhexyl alcohol (104-76-7) + 2,5-diiodo-1,4-dibenzoic acid (20856-80-8) → bis(2-ethylhexyl) 2,5-diiodoterephthalate (935271-96-8)

Guidance literature:

With sulfuric acid; In toluene; for 24h; Reflux;

DOI:10.1002/adfm.201102027

Reference yield:

2,5-diiodo-4-methylbenzoic acid (20856-79-5) → bis(2-ethylhexyl) 2,5-diiodoterephthalate (935271-96-8)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium permanganate; potassium hydroxide

2: sulfuric acid / toluene / 24 h / Reflux

With potassium permanganate; sulfuric acid; potassium hydroxide; In toluene;

DOI:10.1002/adfm.201102027

upstream raw materials:

2-Ethylhexyl alcohol

2,5-diiodo-1,4-dibenzoic acid

2,5-diiodo-4-methylbenzoic acid