diphenylmethyl 2-(3-diphenylmethoxy-4-pyridon-1-yl)-4-hydroxybutyrate

Base Information

Chemical Name:diphenylmethyl 2-(3-diphenylmethoxy-4-pyridon-1-yl)-4-hydroxybutyrate
CAS No.:138456-41-4
Molecular Formula:C₃₅H₃₁NO₅
Molecular Weight:545.635
Hs Code.:

Synonyms:

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Chemical Property of diphenylmethyl 2-(3-diphenylmethoxy-4-pyridon-1-yl)-4-hydroxybutyrate

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Technology Process of diphenylmethyl 2-(3-diphenylmethoxy-4-pyridon-1-yl)-4-hydroxybutyrate

There total 1 articles about diphenylmethyl 2-(3-diphenylmethoxy-4-pyridon-1-yl)-4-hydroxybutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131580-89-7
3-Diphenylmethoxy-4-pyrone

: 138456-41-4
diphenylmethyl 2-(3-diphenylmethoxy-4-pyridon-1-yl)-4-hydroxybutyrate

Guidance literature:: Multi-step reaction with 2 steps

1: 530 mg / NaOH / H₂O; methanol / 10 h / 80 °C

2: 1) 5percent HCl / 1) water, 5 deg C, 2) CH₂Cl₂, 1 h

With hydrogenchloride; sodium hydroxide; In methanol; water;
DOI:10.1248/cpb.38.3476

Reference yield:

: 138456-41-4
diphenylmethyl 2-(3-diphenylmethoxy-4-pyridon-1-yl)-4-hydroxybutyrate

: 133076-24-1
4-Aminooxy-2-(3-benzhydryloxy-4-oxo-4H-pyridin-1-yl)-butyric acid benzhydryl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 624 mg / triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 1 h / 5 °C

2: hydrazine monohydrate / CH₂Cl₂ / 1 h / 5 °C

With hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane;
DOI:10.1248/cpb.38.3476

Reference yield:

: 138456-41-4
diphenylmethyl 2-(3-diphenylmethoxy-4-pyridon-1-yl)-4-hydroxybutyrate

: 133076-23-0
(Z)-2-(2-tritylaminothiazol-4-yl)-2-<3-(3-diphenylmethoxy-4-pyridon-1-yl)-3-diphenylmethoxycarbonylpropoxyimino>acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 624 mg / triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 1 h / 5 °C

2: hydrazine monohydrate / CH₂Cl₂ / 1 h / 5 °C

3: 580 mg / ethanol; CHCl₃ / 17 h / Ambient temperature

With hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane; chloroform;
DOI:10.1248/cpb.38.3476