di-(2-nitrobenzyl) 3β-4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)>-2β-hydroxy-Δ¹²-oleanene-23,28-dioate

Base Information

• Chemical Name: di-(2-nitrobenzyl) 3β-4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)>-2β-hydroxy-Δ¹²-oleanene-23,28-dioate
• CAS No.: 124857-55-2
• Molecular Formula: C₇₀H₉₀N₂O₂₇
• Molecular Weight: 1391.48

Synonyms:

Chemical Property of di-(2-nitrobenzyl) 3β-4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)>-2β-hydroxy-Δ¹²-oleanene-23,28-dioate

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Technology Process of di-(2-nitrobenzyl) 3β-4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)>-2β-hydroxy-Δ¹²-oleanene-23,28-dioate

There total 1 articles about di-(2-nitrobenzyl) 3β-4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)>-2β-hydroxy-Δ¹²-oleanene-23,28-dioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

di-(2-nitrobenzyl) 2β,3β-dihydroxy-Δ12-oleanene-23,28-dioate (124857-54-1) + 2,3,6,2',3',4',6'-hepta-O-acetyl-α-D-maltosyl bromide (4753-07-5,5160-10-1,14206-57-6,14227-66-8,14257-35-3,42385-75-1,67650-37-7,68682-05-3,69308-57-2,69349-74-2,70223-96-0,70223-97-1,71276-38-5,85248-99-3,118493-15-5,120575-76-0) → di-(2-nitrobenzyl) 3β-4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)>-2β-hydroxy-Δ12-oleanene-23,28-dioate (124857-55-2)

Guidance literature:

With silver perchlorate; silver carbonate; In benzene; for 3h; Heating;

DOI:10.1016/0008-6215(89)85111-0

upstream raw materials:

di-(2-nitrobenzyl) 2β,3β-dihydroxy-Δ¹²-oleanene-23,28-dioate

2,3,6,2',3',4',6'-hepta-O-acetyl-α-D-maltosyl bromide

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