C₁₅H₁₃FO₃S

Base Information

• Chemical Name: C₁₅H₁₃FO₃S
• CAS No.: 1393639-42-3
• Molecular Formula: C₁₅H₁₃FO₃S
• Molecular Weight: 292.331
• Mol file: 1393639-42-3.mol

Synonyms:

Chemical Property of C₁₅H₁₃FO₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₃FO₃S

There total 4 articles about C₁₅H₁₃FO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[2-(4-fluorophenoxy)phenyl]methanol (70764-39-5) → C15H13FO3S (1393639-42-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: hydrogen bromide / water / 0.5 h / Reflux

2.1: sodium hydroxide / 1 h / 80 °C

2.2: 2 h / Reflux

With hydrogen bromide; sodium hydroxide; In water;

DOI:10.1016/j.ejmech.2012.05.038

Reference yield:

2-(4-fluorophenoxy)benzaldehyde (320423-61-8) → C15H13FO3S (1393639-42-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate; isopropyl alcohol / 20 °C

2.1: hydrogen bromide / water / 0.5 h / Reflux

3.1: sodium hydroxide / 1 h / 80 °C

3.2: 2 h / Reflux

With sodium tetrahydroborate; hydrogen bromide; isopropyl alcohol; sodium hydroxide; In water;

DOI:10.1016/j.ejmech.2012.05.038

Reference yield:

2-Fluorobenzaldehyde (446-52-6) → C15H13FO3S (1393639-42-3)

Guidance literature:

Multi-step reaction with 4 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / Reflux

2.1: sodium tetrahydroborate; isopropyl alcohol / 20 °C

3.1: hydrogen bromide / water / 0.5 h / Reflux

4.1: sodium hydroxide / 1 h / 80 °C

4.2: 2 h / Reflux

With sodium tetrahydroborate; hydrogen bromide; caesium carbonate; isopropyl alcohol; sodium hydroxide; In water; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2012.05.038

upstream raw materials:

C₁₄H₁₃FN₂OS

chloroacetic acid

[2-(4-fluorophenoxy)phenyl]methanol

2-Fluorobenzaldehyde

Downstream raw materials:

C₁₅H₁₄FNO₂S

Refernces