phenylspirocycloheptene>

Base Information

• Chemical Name: phenylspirocycloheptene>
• CAS No.: 101220-50-2
• Molecular Formula: C₂₃H₂₀
• Molecular Weight: 296.412
• Mol file: 101220-50-2.mol

Synonyms:

Chemical Property of phenylspirocycloheptene>

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenylspirocycloheptene>

There total 2 articles about phenylspirocycloheptene> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.1%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 5-diazo-10,11-dihydro-5H-dibenzo[a,d]cycloheptene (6141-55-5) → 10,10’,11,11’-tetrahydro-5H,5’H-5,5’-bidibenzo[a,d][7]annulene (15323-21-4) + phenylspirocycloheptene> (101220-50-2)

Guidance literature:

at 25 ℃; for 1.5h; Irradiation;

DOI:10.1021/jo00379a023

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 10,11-dihydrodibenzocycloheptadien-5-ylidene (15306-40-8) → phenylspirocycloheptene> (101220-50-2)

Guidance literature:

In benzene; Rate constant;

DOI:10.1021/jo00379a023

upstream raw materials:

styrene

10,11-dihydrodibenzocycloheptadien-5-ylidene

5-diazo-10,11-dihydro-5H-dibenzo[a,d]cycloheptene