Ethyl 17-Benzoxyheptadecanoat

Base Information

• Chemical Name: Ethyl 17-Benzoxyheptadecanoat
• CAS No.: 53821-24-2
• Molecular Formula: C₂₆H₄₄O₃
• Molecular Weight: 404.634
• Mol file: 53821-24-2.mol

Synonyms:

Chemical Property of Ethyl 17-Benzoxyheptadecanoat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ethyl 17-Benzoxyheptadecanoat

There total 3 articles about Ethyl 17-Benzoxyheptadecanoat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

11-bromoundecanoic acid (2834-05-1) → Ethyl 17-Benzoxyheptadecanoat (53821-24-2)

Guidance literature:

Multi-step reaction with 3 steps

1: NaI / acetone / 12 h / Heating

2: H₂SO₄ / toluene

3: (i) CuI, MeLi, THF, Et₂O, (ii) /BRN= 1774696/

With sulfuric acid; sodium iodide; In acetone; toluene;

DOI:10.1021/jo00894a605

Reference yield:

11-iodo-undecanoic acid (63632-65-5) → Ethyl 17-Benzoxyheptadecanoat (53821-24-2)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂SO₄ / toluene

2: (i) CuI, MeLi, THF, Et₂O, (ii) /BRN= 1774696/

With sulfuric acid; In toluene;

DOI:10.1021/jo00894a605

Reference yield:

ethyl 11-iodoundecanoate (53821-20-8) + 6-benzyloxyhexylmagnesium chloride → Ethyl 17-Benzoxyheptadecanoat (53821-24-2)

Guidance literature:

Multistep reaction; (i) CuI, MeLi, THF, Et₂O, (ii) /BRN= 1774696/;

DOI:10.1021/jo00894a605

upstream raw materials:

ethyl 11-iodoundecanoate

11-bromoundecanoic acid

11-iodo-undecanoic acid