Technology Process of C10H10(18)FNO2
There total 3 articles about C10H10(18)FNO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C
2.2: 4 h / 20 °C
3.1: C18H36N2O6*(19)F(1-)*K(1+); 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / N,N-dimethyl-formamide / 120 °C
4.1: trifluoroacetic acid / water; N,N-dimethyl-formamide / 0.08 h / 20 °C
With
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; C18H36N2O6*(19)F(1-)*K(1+); 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;
In
dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.3900
- Guidance literature:
-
Multi-step reaction with 2 steps
1: C18H36N2O6*(19)F(1-)*K(1+); 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / N,N-dimethyl-formamide / 120 °C
2: trifluoroacetic acid / water; N,N-dimethyl-formamide / 0.08 h / 20 °C
With
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; C18H36N2O6*(19)F(1-)*K(1+); trifluoroacetic acid;
In
water; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.3900
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C
1.2: 4 h / 20 °C
2.1: C18H36N2O6*(19)F(1-)*K(1+); 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / N,N-dimethyl-formamide / 120 °C
3.1: trifluoroacetic acid / water; N,N-dimethyl-formamide / 0.08 h / 20 °C
With
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; C18H36N2O6*(19)F(1-)*K(1+); 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;
In
dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.3900
