Technology Process of C33H45N3O13S
There total 9 articles about C33H45N3O13S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: methanol; di(n-butyl)tin oxide / 55 °C
2: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide
With
methanol; sulfur trioxide trimethylamine complex; di(n-butyl)tin oxide;
In
N,N-dimethyl-formamide;
DOI:10.1021/ac5004135
- Guidance literature:
-
Multi-step reaction with 7 steps
1: water / 100 °C
2: isopropyl alcohol / water / 65 °C
3: Alkaline conditions
4: 2,6-di-tert-butyl-4-methylpyridine; boron trifluoride diethyl etherate / dichloromethane
5: sodium methylate; methanol
6: methanol; di(n-butyl)tin oxide / 55 °C
7: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide
With
methanol; 2,6-di-tert-butyl-4-methylpyridine; boron trifluoride diethyl etherate; water; sodium methylate; sulfur trioxide trimethylamine complex; di(n-butyl)tin oxide; isopropyl alcohol;
In
dichloromethane; water; N,N-dimethyl-formamide;
2: |Michael Addition;
DOI:10.1021/ac5004135
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium hydrogencarbonate / dichloromethane; water
2: isopropyl alcohol / water / 65 °C
3: Alkaline conditions
4: 2,6-di-tert-butyl-4-methylpyridine; boron trifluoride diethyl etherate / dichloromethane
5: sodium methylate; methanol
6: methanol; di(n-butyl)tin oxide / 55 °C
7: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide
With
methanol; 2,6-di-tert-butyl-4-methylpyridine; boron trifluoride diethyl etherate; sodium methylate; sulfur trioxide trimethylamine complex; di(n-butyl)tin oxide; sodium hydrogencarbonate; isopropyl alcohol;
In
dichloromethane; water; N,N-dimethyl-formamide;
2: |Michael Addition;
DOI:10.1021/ac5004135