1-Hydroxy-2--1,2-diphenylethyl diphenylphosphinodithioate

Base Information

• Chemical Name: 1-Hydroxy-2--1,2-diphenylethyl diphenylphosphinodithioate
• CAS No.: 134225-83-5
• Molecular Formula: C₃₂H₂₆NOPS₂
• Molecular Weight: 535.67
• Mol file: 134225-83-5.mol

Synonyms:

Chemical Property of 1-Hydroxy-2--1,2-diphenylethyl diphenylphosphinodithioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Hydroxy-2--1,2-diphenylethyl diphenylphosphinodithioate

There total 1 articles about 1-Hydroxy-2--1,2-diphenylethyl diphenylphosphinodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

α-phenylimino-deoxybenzoin (4198-95-2) + diphenylphosphinodithioic acid (1015-38-9) → 1-Hydroxy-2--1,2-diphenylethyl diphenylphosphinodithioate (134225-83-5)

Guidance literature:

In benzene; for 12h; Heating;

Reference yield: 85.0%

1-Hydroxy-2--1,2-diphenylethyl diphenylphosphinodithioate (134225-83-5) → α-phenylimino-deoxybenzoin (4198-95-2)

Guidance literature:

With sodium hydroxide; for 1h; Ambient temperature;

Reference yield:

1-Hydroxy-2--1,2-diphenylethyl diphenylphosphinodithioate (134225-83-5) → 1-Hydroxy-2--1,2-diphenylethyl thiophenol-2-amino (134225-82-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / 10percent aq. NaOH / 1 h / Ambient temperature

2: 70 percent / toluene / Heating

With sodium hydroxide; In toluene;

upstream raw materials:

α-phenylimino-deoxybenzoin

diphenylphosphinodithioic acid

Downstream raw materials:

α-phenylimino-deoxybenzoin

1-Hydroxy-2--1,2-diphenylethyl thiophenol-2-amino