Technology Process of 2-Cyclohex-3-enylmethylene-[1,3]dithiane
There total 1 articles about 2-Cyclohex-3-enylmethylene-[1,3]dithiane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) 15percent methanol. HCl, 2.) 1 M aq. NaOH / 1.) reflux, 2.) reflux
2: 87 percent / I2, KI, NaHCO3 / H2O
3: 58 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / toluene
4: 96 percent / methanol / 100 °C
5: 70 percent / lithium aluminum hydride (LAH) / tetrahydrofuran
With
hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; iodine; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium iodide;
In
tetrahydrofuran; methanol; water; toluene;
DOI:10.1039/c39920000795
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) 15percent methanol. HCl, 2.) 1 M aq. NaOH / 1.) reflux, 2.) reflux
2: 87 percent / I2, KI, NaHCO3 / H2O
3: 58 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / toluene
4: 96 percent / methanol / 100 °C
With
hydrogenchloride; sodium hydroxide; iodine; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium iodide;
In
methanol; water; toluene;
DOI:10.1039/c39920000795
