1-propyl-cyclohexanecarboxylic acid amide

Base Information

• Chemical Name: 1-propyl-cyclohexanecarboxylic acid amide
• CAS No.: 99175-66-3
• Molecular Formula: C₁₀H₁₉NO
• Molecular Weight: 169.267
• Mol file: 99175-66-3.mol

Synonyms:

Chemical Property of 1-propyl-cyclohexanecarboxylic acid amide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-propyl-cyclohexanecarboxylic acid amide

There total 12 articles about 1-propyl-cyclohexanecarboxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenyl-(1-propyl-cyclohexyl)-ketone → 1-propyl-cyclohexanecarboxylic acid amide (99175-66-3)

Guidance literature:

With sodium amide; toluene;

DOI:10.1021/ja01098a033

Reference yield:

Cyclohexyl phenyl ketone (712-50-5) → 1-propyl-cyclohexanecarboxylic acid amide (99175-66-3)

Guidance literature:

Multi-step reaction with 2 steps

1: NaNH₂; toluene / anschliessend Erwaermen mit Propyljodid

2: NaNH₂; toluene

With sodium amide; toluene;

DOI:10.1021/ja01098a033

Reference yield:

1-methyl-1-cyclohexanecarboxylic acid (1123-25-7) → 1-propyl-cyclohexanecarboxylic acid amide (99175-66-3)

Guidance literature:

Multi-step reaction with 5 steps

1: lithium alanate; diethyl ether

2: formic acid; H₂SO₄

3: lithium alanate

4: H₂SO₄

With lithium aluminium tetrahydride; formic acid; diethyl ether; sulfuric acid;

upstream raw materials:

1-propyl-cyclohexanecarboxylic acid

1-methyl-1-cyclohexanecarboxylic acid

1-ethylcyclohexane-1-carboxylic acid

cycloheptanol

Downstream raw materials:

1-propyl-cyclohexylamine