3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (10S,11R)-10-(3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-8,9,10,11-tetrahydro-benzo[a]anthracen-11-yl ester

Base Information

• Chemical Name: 3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (10S,11R)-10-(3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-8,9,10,11-tetrahydro-benzo[a]anthracen-11-yl ester
• CAS No.: 91365-99-0
• Molecular Formula: C₃₈H₃₀F₆O₆
• Molecular Weight: 696.643

Synonyms:

Chemical Property of 3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (10S,11R)-10-(3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-8,9,10,11-tetrahydro-benzo[a]anthracen-11-yl ester

Chemical Property:

Purity/Quality:

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Technology Process of 3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (10S,11R)-10-(3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-8,9,10,11-tetrahydro-benzo[a]anthracen-11-yl ester

There total 2 articles about 3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (10S,11R)-10-(3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-8,9,10,11-tetrahydro-benzo[a]anthracen-11-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

(-)-methoxytrifluoromethylphenylacetyl chloride (39637-99-5) + 10,11-Dihydroxy-8,9,10,11-tetrahydroanthracene (79252-28-1,91384-62-2,94903-89-6) → 3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (10R,11S)-10-(3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-8,9,10,11-tetrahydro-benzo[a]anthracen-11-yl ester (91422-89-8) + 3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (10S,11R)-10-(3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-8,9,10,11-tetrahydro-benzo[a]anthracen-11-yl ester (91365-99-0)

Guidance literature:

In pyridine; 1) 0 deg C, 2 h, 2) ambient temperature, 10 h;

DOI:10.1021/jo00193a033

Reference yield:

(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride (39637-99-5,20445-33-4) + (+)-cis-(10S,11R)-10,11-Dihydroxy-8,9,10,11-tetrahydrobenzanthracene (91384-62-2) → (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (10S,11R)-10-((R)-3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-8,9,10,11-tetrahydro-benzo[a]anthracen-11-yl ester (91365-99-0)

Guidance literature:

With pyridine; for 16h; Yield given; Ambient temperature;

DOI:10.1016/S0040-4039(00)91907-5

Reference yield: 80.0%

3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (10S,11R)-10-(3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-8,9,10,11-tetrahydro-benzo[a]anthracen-11-yl ester (91365-99-0) → (+)-cis-(10S,11R)-10,11-Dihydroxy-8,9,10,11-tetrahydrobenzanthracene (91384-62-2)

Guidance literature:

With methanol; sodium hydroxide; In tetrahydrofuran; for 24h; Ambient temperature;

DOI:10.1021/jo00193a033

upstream raw materials:

(-)-methoxytrifluoromethylphenylacetyl chloride

10,11-Dihydroxy-8,9,10,11-tetrahydroanthracene

(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride

(+)-cis-(10S,11R)-10,11-Dihydroxy-8,9,10,11-tetrahydrobenzanthracene

Downstream raw materials:

(+)-cis-(10S,11R)-10,11-Dihydroxy-8,9,10,11-tetrahydrobenzanthracene

C₃₂H₂₄O₄

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