(1R,2R)-1,2-Diphenyl-O-(2',3'-epoxy)-propylglycerol

Base Information

Chemical Name:(1R,2R)-1,2-Diphenyl-O-(2',3'-epoxy)-propylglycerol
CAS No.:145626-45-5
Molecular Formula:C₁₇H₁₈O₃
Molecular Weight:270.328
Hs Code.:

Synonyms:

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Chemical Property of (1R,2R)-1,2-Diphenyl-O-(2',3'-epoxy)-propylglycerol

Chemical Property:

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Technology Process of (1R,2R)-1,2-Diphenyl-O-(2',3'-epoxy)-propylglycerol

There total 2 articles about (1R,2R)-1,2-Diphenyl-O-(2',3'-epoxy)-propylglycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 145626-44-4
(1R,2R)-O-(2'-Propenyl)-1,2-diphenyl-1,2-ethanediol

: 145626-45-5,145679-74-9
(1R,2R)-1,2-Diphenyl-O-(2',3'-epoxy)-propylglycerol

Guidance literature:: With 6,6'-di-tert-butyl-4,4'-thiodi-o-cresol; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1) reflux, 1 h, b) r.t., 16 h;
DOI:10.1016/S0040-4020(01)92276-8

Reference yield:

: 52340-78-0
(R,R)-hydroxybenzoin

: 145626-45-5,145679-74-9
(1R,2R)-1,2-Diphenyl-O-(2',3'-epoxy)-propylglycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) n-Bu₂SnO, 2) CsF / 1) benzene, 60 deg C, 2) DMF, a) 60 deg C, 1 h, b) r.t., 16 h

2: 74 percent / m-CPBA, 3-tert-butyl-4-hydroxy-5-methylphenyl sulfide / CH₂Cl₂ / 1) reflux, 1 h, b) r.t., 16 h

With 6,6'-di-tert-butyl-4,4'-thiodi-o-cresol; di(n-butyl)tin oxide; 3-chloro-benzenecarboperoxoic acid; cesium fluoride; In dichloromethane;
DOI:10.1016/S0040-4020(01)92276-8

Reference yield:

: 145626-45-5,145679-74-9
(1R,2R)-1,2-Diphenyl-O-(2',3'-epoxy)-propylglycerol

: 145626-54-6,145626-63-7,145626-65-9,145626-67-1
1-((2R,5R,6R)-5,6-Diphenyl-[1,4]dioxan-2-yl)-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: (+)-camphorsulfonic acid / CH₂Cl₂ / 3 h / Heating

2: 1) oxalyl chloride, DMSO, 2) NEt₃ / 1) CH₂Cl₂, -35 deg C, 15 min, 2) up to r.t.

With oxalyl dichloride; dimethyl sulfoxide; (+)-10-camphorsulfonic acid; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4020(01)92276-8