(-)-shikimate 3-phosphate trisodium salt

Base Information

• Chemical Name: (-)-shikimate 3-phosphate trisodium salt
• CAS No.: 93060-75-4
• Molecular Formula: C₇H₈O₈P*3Na
• Molecular Weight: 320.079
• Mol file: 93060-75-4.mol

Synonyms:

Chemical Property of (-)-shikimate 3-phosphate trisodium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (-)-shikimate 3-phosphate trisodium salt

There total 15 articles about (-)-shikimate 3-phosphate trisodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

Methyl 4,5-O-diacetyl-(-)-shikimate 3-phosphate (1053643-69-8) → (-)-shikimate 3-phosphate trisodium salt (93060-75-4,143393-03-7)

Guidance literature:

With sodium hydroxide; at 0 ℃; for 3h;

DOI:10.1021/jo00047a049

Reference yield: 76.0%

(2S,3S,4aR,8R,8aS)-8-(Bis-benzyloxy-phosphoryloxy)-2,3-dimethoxy-2,3-dimethyl-2,3,4a,5,8,8a-hexahydro-benzo[1,4]dioxine-6-carboxylic acid methyl ester (282535-08-4) → (-)-shikimate 3-phosphate trisodium salt (93060-75-4,143393-03-7)

Guidance literature:

(2S,3S,4aR,8R,8aS)-8-(Bis-benzyloxy-phosphoryloxy)-2,3-dimethoxy-2,3-dimethyl-2,3,4a,5,8,8a-hexahydro-benzo[1,4]dioxine-6-carboxylic acid methyl ester; With trimethylsilyl bromide; In dichloromethane;

With sodium hydroxide;

DOI:10.1016/S0040-4039(00)00280-X

Reference yield: 47.0%

shikimic acid (138-59-0) → (-)-shikimate 3-phosphate trisodium salt (93060-75-4,143393-03-7)

Guidance literature:

With ATP; shikimate kinase, 1.) 6 h, 2.) 13 deg C_., overnight;

DOI:10.1021/jo00017a034

upstream raw materials:

shikimic acid

Methyl 4,5-O-diacetyl-(-)-shikimate 3-phosphate

(2S,3S,4aR,8R,8aS)-8-(Bis-benzyloxy-phosphoryloxy)-2,3-dimethoxy-2,3-dimethyl-2,3,4a,5,8,8a-hexahydro-benzo[1,4]dioxine-6-carboxylic acid methyl ester

methyl shikimate