meso-2,2'-<(1,2-diphenylethylene)bis(iminomethylene)>diphenol

Base Information

Chemical Name:meso-2,2'-<(1,2-diphenylethylene)bis(iminomethylene)>diphenol
CAS No.:84995-07-3
Molecular Formula:C₂₈H₂₈N₂O₂
Molecular Weight:424.543
Hs Code.:

Synonyms:

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Chemical Property of meso-2,2'-<(1,2-diphenylethylene)bis(iminomethylene)>diphenol

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Technology Process of meso-2,2'-<(1,2-diphenylethylene)bis(iminomethylene)>diphenol

There total 1 articles about meso-2,2'-<(1,2-diphenylethylene)bis(iminomethylene)>diphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 41013-29-0,51208-40-3,58520-13-1,61045-68-9,61045-69-0,132295-13-7,41013-30-3
N,N'-disalicylidene-(R,S)(S,R)-1,2-diphenyl-1,2-ethanediamine

: 84995-07-3
meso-2,2'-<(1,2-diphenylethylene)bis(iminomethylene)>diphenol

Guidance literature:: With pyridine; sodium tetrahydroborate;
DOI:10.1246/bcsj.56.99

Reference yield: 42.0%

: 6018-89-9
nickel(II) acetate tetrahydrate

: 84995-07-3
meso-2,2'-<(1,2-diphenylethylene)bis(iminomethylene)>diphenol

: [Ni(OC₆H₄CHNCH(C₆H₅)CH(C₆H₅)NHCH₂C₆H₄O)(C₅H₅N)]

Guidance literature:: With pyridine; sodium hydroxide; air; In methanol; water; acetone; to soln. of ligand in acetone added Ni(OAc)2*4H2O in methanol, 20% aq. NaOH soln. added dropwise, left standing overnight at room temp., air bubbled through soln. for 5 h at room temp.; concd. by air bubbling, ppt. collected by filtration, washed with water, dissolved in methanol, filtered, evapd., recrystd. from pyridine-water; elem. anal.;
DOI:10.1246/bcsj.56.99

Reference yield: 13.0%

: 6018-89-9
nickel(II) acetate tetrahydrate

: 84995-07-3
meso-2,2'-<(1,2-diphenylethylene)bis(iminomethylene)>diphenol

: [Ni((OC₆H₄CHNCHC₆H₅)2)]

: 84973-99-9
[2,2'-((cis-1,2-diphenylethenylene)bis(nitrilomethylidyne))diphenolato]nickel(II)

Guidance literature:: With air; In pyridine; educts dissolved in pyridine, heated on water bath for 30 h, cooled; crystd. by adding methanol, ppt. filtered, washed with methanol, filtrate stood overnight at room temp.; elem. anal.;
DOI:10.1246/bcsj.56.99