[W(C₅H₅)2H(SC₆H₅)]

Base Information

Chemical Name:[W(C₅H₅)2H(SC₆H₅)]
CAS No.:83526-25-4
Molecular Formula:C₁₆H₁₆SW
Molecular Weight:424.219
Hs Code.:

[W(C<sub>5</sub>H<sub>5</sub>)2H(SC<sub>6</sub>H<sub>5</sub>)]

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Suppliers and Price of [W(C₅H₅)2H(SC₆H₅)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [W(C₅H₅)2H(SC₆H₅)]

Chemical Property:

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Technology Process of [W(C₅H₅)2H(SC₆H₅)]

There total 2 articles about [W(C₅H₅)2H(SC₆H₅)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 16853-85-3
lithium aluminium tetrahydride

: 12246-20-7
W(η5-C5H5)2(SC6H5)2

: 83526-25-4
[W(C₅H₅)2H(SC₆H₅)]

Guidance literature:: In tetrahydrofuran; under N2, suspn. of W complex in dry THF treated at room temp. with LiAlH4 for 30 min; evapd. below 25°C, cold ethanol added, evapd., extd. with toluene, evapd., pentane added; elem. anal.;
DOI:10.1016/S0022-328X(00)82702-3

Reference yield:

: 16940-66-2
sodium tetrahydroborate

: 12246-20-7
W(η5-C5H5)2(SC6H5)2

: 83526-25-4
[W(C₅H₅)2H(SC₆H₅)]

Guidance literature:: In tetrahydrofuran; water; under N2, suspn. of W complex in THF/water treated with large excess ofNaBH4 at 50°C for 4 h; evapd., extd. with warm toluene, concd., recrystd. from toluene; elem. anal.;
DOI:10.1016/S0022-328X(00)82702-3