C₂H₂B₁₀H₇(CCC₆H₅)(CH₃)2

Base Information

Chemical Name:C₂H₂B₁₀H₇(CCC₆H₅)(CH₃)2
CAS No.:98458-07-2
Molecular Formula:C₁₂H₂₀B₁₀
Molecular Weight:272.401
Hs Code.:

C<sub>2</sub>H<sub>2</sub>B<sub>10</sub>H<sub>7</sub>(CCC<sub>6</sub>H<sub>5</sub>)(CH<sub>3</sub>)2

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Chemical Property of C₂H₂B₁₀H₇(CCC₆H₅)(CH₃)2

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Technology Process of C₂H₂B₁₀H₇(CCC₆H₅)(CH₃)2

There total 1 articles about C₂H₂B₁₀H₇(CCC₆H₅)(CH₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 20347-47-1
1,2-dimethyl-9-iodo-1,2-dicarba-closo-dodecaborane

: 925-90-6
ethylmagnesium bromide

: 536-74-3
phenylacetylene

: 98458-07-2
C₂H₂B₁₀H₇(CCC₆H₅)(CH₃)2

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; diethyl ether; addn. of EtMgBr in ether to a soln. of acetylenic derivate in absolute dioxane (N2), heating for 1 h at 40°C, cooling, addn. of carborane and Pd-catalyst in dioxane, heating for 30 h at 60°C (stirring), monitoring of react. by GLC; pouring into a ca. 18% soln. of HCl, extn. by ether, washing with H2O, drying (MgSO4), distn. of solvents in vac., column chromy. of residue (silica gel), benzene-petroleum ether (bp 40-70°C) as eluent; elem.anal.;
DOI:10.1007/BF00948065