3-thiobenzoyl-2-phenyl-5,6-dihydrobenzo-2H-thiochromene

Base Information

Chemical Name:3-thiobenzoyl-2-phenyl-5,6-dihydrobenzo-2H-thiochromene
CAS No.:118210-65-4
Molecular Formula:C₂₆H₂₀S₂
Molecular Weight:396.577
Hs Code.:

3-thiobenzoyl-2-phenyl-5,6-dihydrobenzo<h>-2H-thiochromene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-thiobenzoyl-2-phenyl-5,6-dihydrobenzo-2H-thiochromene

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Technology Process of 3-thiobenzoyl-2-phenyl-5,6-dihydrobenzo-2H-thiochromene

There total 2 articles about 3-thiobenzoyl-2-phenyl-5,6-dihydrobenzo-2H-thiochromene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 118210-64-3
3-benzoyl-2-phenyl-5,6-dihydrobenzo-2H-thiochromene

: 118210-65-4
3-thiobenzoyl-2-phenyl-5,6-dihydrobenzo-2H-thiochromene

Guidance literature:: In carbon disulfide; for 5h; Heating;
DOI:10.1246/bcsj.63.2540

Reference yield:

: 118210-62-1
3-benzoyl-3,4,5,6-tetrahydro-2-phenyl-4-phenylthio-2H-naphtho<1,2-b>thiin

: 118210-65-4
3-thiobenzoyl-2-phenyl-5,6-dihydrobenzo-2H-thiochromene

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / sodium ethoxide / benzene; ethanol / Ambient temperature

2: 55 percent / Lawesson reagent / CS₂ / 5 h / Heating

With Lawessons reagent; sodium ethanolate; In carbon disulfide; ethanol; benzene;
DOI:10.1246/cl.1988.1029