C₂₉H₂₉Cl₂N₅O₁₀

Base Information

Chemical Name:C₂₉H₂₉Cl₂N₅O₁₀
CAS No.:1438408-42-4
Molecular Formula:C₂₉H₂₉Cl₂N₅O₁₀
Molecular Weight:678.483
Hs Code.:

C<sub>29</sub>H<sub>29</sub>Cl<sub>2</sub>N<sub>5</sub>O<sub>10</sub>

Synonyms:

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Chemical Property of C₂₉H₂₉Cl₂N₅O₁₀

Chemical Property:

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Technology Process of C₂₉H₂₉Cl₂N₅O₁₀

There total 15 articles about C₂₉H₂₉Cl₂N₅O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1438408-41-3
C₂₆H₂₃Cl₂N₅O₁₀

: 18107-18-1
diazomethyl-trimethyl-silane

: 1438408-42-4
C₂₉H₂₉Cl₂N₅O₁₀

Guidance literature:: In methanol; toluene; at 0 ℃; Inert atmosphere;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-17-3
C₁₄H₂₄INO₃

: 1438408-42-4
C₂₉H₂₉Cl₂N₅O₁₀

Guidance literature:: Multi-step reaction with 13 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Cooling with ice; Inert atmosphere

1.2: 8 h / 20 °C / Inert atmosphere

1.3: 3.33 h / 20 °C / Inert atmosphere

2.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

4.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

5.1: sodium hydrogencarbonate; mercuric triflate / dichloromethane / 10.5 h / -20 °C / Inert atmosphere; Cooling with ice

5.2: 0.5 h / -78 °C / Inert atmosphere

6.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

7.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10.33 h / -40 - -20 °C / Inert atmosphere

8.1: Trimethyl borate / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere

8.2: 3 h / 50 °C / Inert atmosphere

9.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / Cooling with ice; Inert atmosphere

9.2: Inert atmosphere

10.1: hydrogenchloride / methanol / 10 h / 40 °C / Inert atmosphere

10.2: 0.5 h / 0 °C / Inert atmosphere

11.1: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / dichloromethane

11.2: 0 - 20 °C / Inert atmosphere

12.1: [bis(acetoxy)iodo]benzene; 2-azatricyclo[3.3.1.1^3,7]dec-2-yloxidanyl / aq. phosphate buffer; acetonitrile / 8 h / 20 °C / pH 6.8 / Inert atmosphere

12.2: 3 h / 20 °C / pH 2 / Inert atmosphere

13.1: methanol; toluene / 0 °C / Inert atmosphere

With hydrogenchloride; 2-azatricyclo[3.3.1.1^3,7]dec-2-yloxidanyl; Trimethyl borate; [bis(acetoxy)iodo]benzene; C₁₅H₂₆Cl₂CuN₂O₂; mercuric triflate; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; aq. phosphate buffer; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil; 3.1: |Dess-Martin Oxidation / 4.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-16-2
C₁₄H₂₅NO₄

: 1438408-42-4
C₂₉H₂₉Cl₂N₅O₁₀

Guidance literature:: Multi-step reaction with 14 steps

1.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / Cooling with ice; Inert atmosphere

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Cooling with ice; Inert atmosphere

2.2: 8 h / 20 °C / Inert atmosphere

2.3: 3.33 h / 20 °C / Inert atmosphere

3.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

5.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; mercuric triflate / dichloromethane / 10.5 h / -20 °C / Inert atmosphere; Cooling with ice

6.2: 0.5 h / -78 °C / Inert atmosphere

7.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

8.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10.33 h / -40 - -20 °C / Inert atmosphere

9.1: Trimethyl borate / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere

9.2: 3 h / 50 °C / Inert atmosphere

10.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / Cooling with ice; Inert atmosphere

10.2: Inert atmosphere

11.1: hydrogenchloride / methanol / 10 h / 40 °C / Inert atmosphere

11.2: 0.5 h / 0 °C / Inert atmosphere

12.1: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / dichloromethane

12.2: 0 - 20 °C / Inert atmosphere

13.1: [bis(acetoxy)iodo]benzene; 2-azatricyclo[3.3.1.1^3,7]dec-2-yloxidanyl / aq. phosphate buffer; acetonitrile / 8 h / 20 °C / pH 6.8 / Inert atmosphere

13.2: 3 h / 20 °C / pH 2 / Inert atmosphere

14.1: methanol; toluene / 0 °C / Inert atmosphere

With 1H-imidazole; hydrogenchloride; 2-azatricyclo[3.3.1.1^3,7]dec-2-yloxidanyl; Trimethyl borate; [bis(acetoxy)iodo]benzene; C₁₅H₂₆Cl₂CuN₂O₂; iodine; mercuric triflate; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; methanol; aq. phosphate buffer; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil; 4.1: |Dess-Martin Oxidation / 5.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d