[(η5-indenyl)Ru(PPh3)(2-pyridylmethyl-2,4-dinitrophenyl ketazine)]PF6

Base Information

Chemical Name:[(η5-indenyl)Ru(PPh3)(2-pyridylmethyl-2,4-dinitrophenyl ketazine)]PF6
CAS No.:866612-65-9
Molecular Formula:C₄₀H₃₃N₅O₄PRu*F₆P
Molecular Weight:924.741
Hs Code.:

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Chemical Property of [(η5-indenyl)Ru(PPh3)(2-pyridylmethyl-2,4-dinitrophenyl ketazine)]PF6

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Technology Process of [(η5-indenyl)Ru(PPh3)(2-pyridylmethyl-2,4-dinitrophenyl ketazine)]PF6

There total 1 articles about [(η5-indenyl)Ru(PPh3)(2-pyridylmethyl-2,4-dinitrophenyl ketazine)]PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 75491-10-0
2-acetylpyridine 2,4-dinitrophenylhydrazone

: 241152-08-9
[(η5-indenyl)(triphenylphosphine)(acetonitrile)ruthenium(II)] hexafluorophosphate

: 866612-65-9
[(η5-indenyl)Ru(PPh3)(2-pyridylmethyl-2,4-dinitrophenyl ketazine)]PF6

Guidance literature:: In dichloromethane; benzene; under N2; a mixt. of Ru-contg. compd. (0.11 mmol) and a ligand (0.22 mmol) were dissolved in a min. amt. of CH2Cl2, and benzene was added; the mixt. was heated to reflux for 10 h; the soln. was evapd. to dryness by rotary evaporator; column chromy. on silica gel (CH2Cl2/acetone, 5:1, v/v as eluent); the soln. was concd. and excess hexane was added; elem. anal.;
DOI:10.1016/j.jorganchem.2005.05.001