2-cyclohexyl-3-(methoxycarbonyl)-5-methoxy-1-methylindole-4,7-dione

Base Information

Chemical Name:2-cyclohexyl-3-(methoxycarbonyl)-5-methoxy-1-methylindole-4,7-dione
CAS No.:192821-01-5
Molecular Formula:C₁₈H₂₁NO₅
Molecular Weight:331.368
Hs Code.:

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Chemical Property of 2-cyclohexyl-3-(methoxycarbonyl)-5-methoxy-1-methylindole-4,7-dione

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Technology Process of 2-cyclohexyl-3-(methoxycarbonyl)-5-methoxy-1-methylindole-4,7-dione

There total 1 articles about 2-cyclohexyl-3-(methoxycarbonyl)-5-methoxy-1-methylindole-4,7-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-Amino-2-cyclohexyl-5-methoxy-1-methyl-1H-indole-3-carboxylic acid methyl ester

: 192821-01-5
2-cyclohexyl-3-(methoxycarbonyl)-5-methoxy-1-methylindole-4,7-dione

Guidance literature:: With disodium hydrogenphosphate; sodium dihydrogenphosphate; potassium nitrososulfonate; In acetone; for 1h; Yield given; Ambient temperature;
DOI:10.1021/jm9608422

Reference yield:

: 192821-01-5
2-cyclohexyl-3-(methoxycarbonyl)-5-methoxy-1-methylindole-4,7-dione

: 2-Cyclohexyl-4,7-dihydroxy-5-methoxy-1-methyl-1H-indole-3-carboxylic acid methyl ester

Guidance literature:: With sodium dithionite; In ethanol; chloroform; for 1h; Ambient temperature;
DOI:10.1021/jm9608422

Reference yield:

: 192821-01-5
2-cyclohexyl-3-(methoxycarbonyl)-5-methoxy-1-methylindole-4,7-dione

: 2-Cyclohexyl-3-hydroxymethyl-5-methoxy-1-methyl-1H-indole-4,7-diol

Guidance literature:: Multi-step reaction with 2 steps

1: aq. Na₂S₂O₄ / CHCl₃; ethanol / 1 h / Ambient temperature

2: LiAlH₄ / tetrahydrofuran / 1 h / 30 °C

With lithium aluminium tetrahydride; sodium dithionite; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1021/jm9608422