Li[Pt(CH2C6H4P(o-tolyl)2-κC,P)(CCPh)2]

Base Information

Chemical Name:Li[Pt(CH2C6H4P(o-tolyl)2-κC,P)(CCPh)2]
CAS No.:934397-29-2
Molecular Formula:C₃₇H₃₀PPt*Li
Molecular Weight:707.64
Hs Code.:

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Chemical Property of Li[Pt(CH2C6H4P(o-tolyl)2-κC,P)(CCPh)2]

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Technology Process of Li[Pt(CH2C6H4P(o-tolyl)2-κC,P)(CCPh)2]

There total 1 articles about Li[Pt(CH2C6H4P(o-tolyl)2-κC,P)(CCPh)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 175720-72-6
[(Pt(CH2C6H4P(o-tolyl)2-κC,P)(μ-Cl))2]

: 536-74-3
phenylacetylene

: 934397-29-2
Li[Pt(CH2C6H4P(o-tolyl)2-κC,P)(CCPh)2]

Guidance literature:: With n-BuLi; In tetrahydrofuran; soln. of BuLi in THF was added to soln. of HCCPh in THF at low temp. (-20°C) under Ar; mixt. was stirred for 15 min; Pt complex was added; reacted at room temp. for 15 h; air-evapd.; CHCl3 added at 0°C; filtered through Celite; evapd.; treated with i-PrOH and hexane; evapd.; hexane added; elem. anal.;
DOI:10.1021/om061102m

Reference yield:

: 934397-29-2
Li[Pt(CH2C6H4P(o-tolyl)2-κC,P)(CCPh)2]

: [Pt(CH2C6H4P(o-tolyl)2-κC,P)(CCPh)2Tl]2

Guidance literature:: Multi-step reaction with 2 steps

1: isopropyl alcohol

2: dichloromethane; methanol

In methanol; dichloromethane; isopropyl alcohol;
DOI:10.1021/om061102m

Reference yield:

: 934397-29-2
Li[Pt(CH2C6H4P(o-tolyl)2-κC,P)(CCPh)2]

: [Pt(CH2C6H4P(o-tolyl)2-κC,P)(CCPh)2Ag]2

Guidance literature:: Multi-step reaction with 2 steps

1: isopropyl alcohol

2: dichloromethane; diethyl ether

In diethyl ether; dichloromethane; isopropyl alcohol;
DOI:10.1021/om061102m