(pentachlorophenyl)-4--2,6-dimethylpiperazin-1-yl>-1,2,5-thiadiazol-3-carboxylate

Base Information

Chemical Name:(pentachlorophenyl)-4--2,6-dimethylpiperazin-1-yl>-1,2,5-thiadiazol-3-carboxylate
CAS No.:129785-64-4
Molecular Formula:C₂₁H₂₁Cl₅N₄O₅S
Molecular Weight:618.753
Hs Code.:

(pentachlorophenyl)-4-<cis-4-<(tert-butoxy)carbonyl>-2,6-dimethylpiperazin-1-yl>-1,2,5-thiadiazol-3-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (pentachlorophenyl)-4--2,6-dimethylpiperazin-1-yl>-1,2,5-thiadiazol-3-carboxylate

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Technology Process of (pentachlorophenyl)-4--2,6-dimethylpiperazin-1-yl>-1,2,5-thiadiazol-3-carboxylate

There total 4 articles about (pentachlorophenyl)-4--2,6-dimethylpiperazin-1-yl>-1,2,5-thiadiazol-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 87-86-5,67471-28-7
Pentachlorophenol

: 129779-31-3
4--2,6-dimethylpiperazin-1-yl>-1,2,5-thiadiazol-3-carbonsaeure

: 129785-64-4
(pentachlorophenyl)-4--2,6-dimethylpiperazin-1-yl>-1,2,5-thiadiazol-3-carboxylate

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; for 14h; Ambient temperature;
DOI:10.1002/hlca.19900730409

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 129785-64-4
(pentachlorophenyl)-4--2,6-dimethylpiperazin-1-yl>-1,2,5-thiadiazol-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / dioxane; H₂O / 1 h / 20 °C

2: 22.5 percent / 2m KOH / CH₂Cl₂; H₂O / 0.5 h / 0 °C / stirring with 10000 rpm in a Waring-Blendor

3: 51 percent / DCC / tetrahydrofuran; CH₂Cl₂ / 14 h / Ambient temperature

With potassium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1002/hlca.19900730409

Reference yield:

: 129779-30-2,1152111-14-2
(3S,5R)-3,5-dimethylpiperazine-1-carboxylic acid tert-butyl ester

: 129785-64-4
(pentachlorophenyl)-4--2,6-dimethylpiperazin-1-yl>-1,2,5-thiadiazol-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 22.5 percent / 2m KOH / CH₂Cl₂; H₂O / 0.5 h / 0 °C / stirring with 10000 rpm in a Waring-Blendor

2: 51 percent / DCC / tetrahydrofuran; CH₂Cl₂ / 14 h / Ambient temperature

With potassium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/hlca.19900730409