3-(2-azidobenzyl)pyridine

Base Information

Chemical Name:3-(2-azidobenzyl)pyridine
CAS No.:78500-80-8
Molecular Formula:C₁₂H₁₀N₄
Molecular Weight:210.238
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-azidobenzyl)pyridine

Chemical Property:

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Technology Process of 3-(2-azidobenzyl)pyridine

There total 6 articles about 3-(2-azidobenzyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78500-75-1
2-aminophenyl-(3-pyridyl)methanol

: 78500-80-8
3-(2-azidobenzyl)pyridine

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / hydrogen, conc. hydrochloric acid / 10percent palladium-charcoal / ethanol / 20 h / Ambient temperature

2: 81 percent / H₂O / 0 °C

3: 66 percent / 30percent hydrogen peroxide / acetic acid / 1.) 55-60 deg C, 2 h, 2.) 75-80 deg C, 15 h

4: 85 percent / 10percent aq. sodium hydroxide / 4 h / Heating

5: 1.) sodium nitrite, conc. HCl 2.) sodium azide / 1.) water

With hydrogenchloride; sodium hydroxide; sodium azide; hydrogen; dihydrogen peroxide; sodium nitrite; palladium on activated charcoal; In ethanol; water; acetic acid;
DOI:10.1039/P19810001132

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 78500-80-8
3-(2-azidobenzyl)pyridine

Guidance literature:: Multi-step reaction with 7 steps

1: 75 percent / n-butyl-lithium / hexane; diethyl ether / 1.) -70 deg C, 2 h, 2.) room temperature, 2 h

2: 98 percent / hydrogen / 10percent palladium-charcoal / aq. ethanol

3: 86 percent / hydrogen, conc. hydrochloric acid / 10percent palladium-charcoal / ethanol / 20 h / Ambient temperature

4: 81 percent / H₂O / 0 °C

5: 66 percent / 30percent hydrogen peroxide / acetic acid / 1.) 55-60 deg C, 2 h, 2.) 75-80 deg C, 15 h

6: 85 percent / 10percent aq. sodium hydroxide / 4 h / Heating

7: 1.) sodium nitrite, conc. HCl 2.) sodium azide / 1.) water

With hydrogenchloride; sodium hydroxide; n-butyllithium; sodium azide; hydrogen; dihydrogen peroxide; sodium nitrite; palladium on activated charcoal; In diethyl ether; ethanol; hexane; water; acetic acid;
DOI:10.1039/P19810001132

Reference yield:

: 78500-77-3
3-(2-aminobenzyl)pyridine

: 78500-80-8
3-(2-azidobenzyl)pyridine

Guidance literature:: With hydrogenchloride; sodium azide; sodium acetate; sodium nitrite; Yield given. Multistep reaction; 1.) water, dioxan, 0 deg C, 30 min, 2.) 0 deg C, 30 min;
DOI:10.1039/P19810001132