diethyl N-glutamate

Base Information

Chemical Name:diethyl N-glutamate
CAS No.:142109-14-6
Molecular Formula:C₃₀H₃₉N₃O₇S
Molecular Weight:585.722
Hs Code.:

diethyl N-<p-(3-benzyloxycarbonyl-2,2-dimethylthiazolidin-4-yl)methylaminobenzoyl>glutamate

Synonyms:

Suppliers and Price of diethyl N-glutamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl N-glutamate

Chemical Property:

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Technology Process of diethyl N-glutamate

There total 6 articles about diethyl N-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(4-{[1-(3-Benzyloxycarbonyl-2,2-dimethyl-thiazolidin-4-yl)-meth-(Z)-ylidene]-amino}-benzoylamino)-pentanedioic acid diethyl ester

: 142109-14-6
diethyl N-glutamate

Guidance literature:: With sodium cyanoborohydride; In ethanol; acetic acid; for 6h; Yield given; Ambient temperature;
DOI:10.1248/cpb.40.49

Reference yield:

: 13726-52-8,34136-22-6
diethyl N-(p-aminobenzoyl)-glutamate

: 142109-14-6
diethyl N-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: glacial AcOH / ethanol / 12 h / Ambient temperature

2: NaBH₃CN / acetic acid; ethanol / 6 h / Ambient temperature

With sodium cyanoborohydride; acetic acid; In ethanol; acetic acid;
DOI:10.1248/cpb.40.49

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 142109-14-6
diethyl N-glutamate

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / NaHCO₃ / ethanol; H₂O / Ambient temperature

2: 83 percent / diisobutyl aluminum hydride (DIBAH) / toluene / 3 h / -78 °C

3: glacial AcOH / ethanol / 12 h / Ambient temperature

4: NaBH₃CN / acetic acid; ethanol / 6 h / Ambient temperature

With diisobutylaluminium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; In ethanol; water; acetic acid; toluene;
DOI:10.1248/cpb.40.49