O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine

Base Information

Chemical Name:O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine
CAS No.:131088-78-3
Molecular Formula:C₅₅H₇₁N₃O₂₆
Molecular Weight:1190.17
Hs Code.:

O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N-<L-aspart-1-oyl-(L-proline)-4-oyl>-β-D-glucopyranosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine

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Technology Process of O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine

There total 21 articles about O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 131088-77-2,131176-19-7
O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine

: 131088-78-3,131176-20-0
O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine

Guidance literature:: With formic acid; for 5h; Ambient temperature;
DOI:10.1016/0008-6215(90)80006-O

Reference yield: 12.1%

: 131088-77-2,131176-19-7
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--α,β-D-glucopyranosylamine

: 131088-78-3,131176-20-0
O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine

: 131088-78-3,131176-20-0
O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine

Guidance literature:: With formic acid; for 5h; Ambient temperature;
DOI:10.1248/cpb.39.2699

Reference yield:

: 87902-12-3
<4-benzyl N-(tert-butoxycarbonyl)-L-aspart-1-oyl>-L-proline methyl ester

: 131088-78-3,131176-20-0
O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / H₂ / 10percent Pd-C / ethanol / 12 h / Ambient temperature

2: 13.2 percent / triethylamine, diethyl cyanophosphonate / tetrahydrofuran / 8 h / Ambient temperature

3: 75 percent / 80percent acetic acid / 3 h / 40 °C

4: 62 percent / Hg(CN)2, 4 Angstroem molecular sieves / nitromethane / 6 h / 55 °C

5: 71 percent / 85percent formic acid / 5 h / Ambient temperature

With formic acid; diethyl cyanophosphonate; 4 A molecular sieve; hydrogen; mercury(II) cyanide; acetic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; nitromethane; ethanol;
DOI:10.1016/0008-6215(90)80006-O