Technology Process of C33H42N6O10
There total 4 articles about C33H42N6O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 99 percent / DEAD; triphenylphosphine / tetrahydrofuran
2: 100 percent / H2 / Pd/C / methanol
3: 45 percent / DEAD; triphenylphosphine / tetrahydrofuran
4: 96 percent / methylamine / tetrahydrofuran
5: 97 percent / tetrahydrofuran
6: 95 percent / aq. LiOH / methanol
7: diisopropylethylamine; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride
With
lithium hydroxide; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; methylamine; diethylazodicarboxylate;
palladium on activated charcoal;
In
tetrahydrofuran; methanol;
1: Mitsunobu reaction / 3: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2004.06.017
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 100 percent / H2 / Pd/C / methanol
2: 45 percent / DEAD; triphenylphosphine / tetrahydrofuran
3: 96 percent / methylamine / tetrahydrofuran
4: 97 percent / tetrahydrofuran
5: 95 percent / aq. LiOH / methanol
6: diisopropylethylamine; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride
With
lithium hydroxide; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; methylamine; diethylazodicarboxylate;
palladium on activated charcoal;
In
tetrahydrofuran; methanol;
2: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2004.06.017
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 97 percent / tetrahydrofuran
2: 95 percent / aq. LiOH / methanol
3: diisopropylethylamine; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride
With
lithium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2004.06.017