N-Boc dihydroanatoxin-a

Base Information

Chemical Name:N-Boc dihydroanatoxin-a
CAS No.:96997-82-9
Molecular Formula:C₁₅H₂₅NO₃
Molecular Weight:267.368
Hs Code.:

Synonyms:

Suppliers and Price of N-Boc dihydroanatoxin-a

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Boc dihydroanatoxin-a

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-Boc dihydroanatoxin-a

There total 25 articles about N-Boc dihydroanatoxin-a which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 111964-10-4,111964-14-8
(E)- and (Z)-t-butyl 2-(1-methoxyethylidene)-9-azabicyclo<4.2.1>nonane-9-carboxylate

: 90741-49-4,90820-98-7,90821-04-8,90821-05-9,96997-82-9,112020-12-9,112020-13-0
N-Boc dihydroanatoxin-a

Guidance literature:: With chloro-trimethyl-silane; sodium iodide; In acetonitrile; for 0.0833333h; Ambient temperature;

Reference yield:

: 112009-92-4
ethyl 2-aminohepta-5,6-dienoate

: 90741-49-4,90820-98-7,90821-04-8,90821-05-9,96997-82-9,112020-12-9,112020-13-0
N-Boc dihydroanatoxin-a

Guidance literature:: Multi-step reaction with 14 steps

1: CH₂Cl₂

2: 88 percent / AgBF₄ / CH₂Cl₂ / 72 h / Ambient temperature

3: CF₃CO₂H / CH₂Cl₂ / Ambient temperature

4: pyridine / 0 °C

5: 1) B₂H₆, 2) aq. NaOH, 30percent aq. H₂O₂ / 1) THF, 20 deg C, 20 min, 2) 30 min, room temp.

6: 63 percent / tetrahydrofuran / 0.17 h / -10 °C

7: 78 percent / PPh₃, 2 M Br₂ / tetrahydrofuran / a) 0 deg C, 10 min, b) up to room temp.

8: 83 percent / NaH / dimethylsulfoxide / 2 h / 40 °C

9: 92 percent / Al-Hg / tetrahydrofuran; H₂O / 3 h / 60 °C

10: 1) LDA / 1) DME, hexane, -78 deg C, 20 min, 2) DME, 5 min

11: NaH / tetrahydrofuran / 14 h / Ambient temperature

12: liquid ammonia, lithium / tetrahydrofuran / 0.05 h / -78 °C

13: methanol / 16 h

14: 65 percent / (CH₃)3SiCl, NaI / acetonitrile / 0.08 h / Ambient temperature

With pyridine; sodium hydroxide; chloro-trimethyl-silane; aluminium amalgam; ammonia; dihydrogen peroxide; bromine; lithium; sodium hydride; triphenylphosphine; trifluoroacetic acid; sodium iodide; diborane; lithium diisopropyl amide; silver tetrafluoroborate; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 112009-90-2
ethyl 2-benzylideneaminohepta-5,6-dienoate

: 90741-49-4,90820-98-7,90821-04-8,90821-05-9,96997-82-9,112020-12-9,112020-13-0
N-Boc dihydroanatoxin-a

Guidance literature:: Multi-step reaction with 15 steps

1: 59 percent / aq. HCl / diethyl ether / 0.67 h / Ambient temperature

2: CH₂Cl₂

3: 88 percent / AgBF₄ / CH₂Cl₂ / 72 h / Ambient temperature

4: CF₃CO₂H / CH₂Cl₂ / Ambient temperature

5: pyridine / 0 °C

6: 1) B₂H₆, 2) aq. NaOH, 30percent aq. H₂O₂ / 1) THF, 20 deg C, 20 min, 2) 30 min, room temp.

7: 63 percent / tetrahydrofuran / 0.17 h / -10 °C

8: 78 percent / PPh₃, 2 M Br₂ / tetrahydrofuran / a) 0 deg C, 10 min, b) up to room temp.

9: 83 percent / NaH / dimethylsulfoxide / 2 h / 40 °C

10: 92 percent / Al-Hg / tetrahydrofuran; H₂O / 3 h / 60 °C

11: 1) LDA / 1) DME, hexane, -78 deg C, 20 min, 2) DME, 5 min

12: NaH / tetrahydrofuran / 14 h / Ambient temperature

13: liquid ammonia, lithium / tetrahydrofuran / 0.05 h / -78 °C

14: methanol / 16 h

15: 65 percent / (CH₃)3SiCl, NaI / acetonitrile / 0.08 h / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; chloro-trimethyl-silane; aluminium amalgam; ammonia; dihydrogen peroxide; bromine; lithium; sodium hydride; triphenylphosphine; trifluoroacetic acid; sodium iodide; diborane; lithium diisopropyl amide; silver tetrafluoroborate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; dimethyl sulfoxide; acetonitrile;