-11-ethoxy-3-(1H-indol-3-ylmethyl)-3-methyl-4,9-dioxo-7-phenyl-12-oxa-2,5,8-triaza-11-phosphatetradecanoic acid 11-oxide tricyclo<3.3.1.1^3,7>dec-2-yl ester

Base Information

• Chemical Name: -11-ethoxy-3-(1H-indol-3-ylmethyl)-3-methyl-4,9-dioxo-7-phenyl-12-oxa-2,5,8-triaza-11-phosphatetradecanoic acid 11-oxide tricyclo<3.3.1.1^3,7>dec-2-yl ester
• CAS No.: 141956-41-4
• Molecular Formula: C₃₇H₄₉N₄O₇P
• Molecular Weight: 692.792

Synonyms:

Chemical Property of -11-ethoxy-3-(1H-indol-3-ylmethyl)-3-methyl-4,9-dioxo-7-phenyl-12-oxa-2,5,8-triaza-11-phosphatetradecanoic acid 11-oxide tricyclo<3.3.1.1^3,7>dec-2-yl ester

Chemical Property:

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Useful:

Technology Process of -11-ethoxy-3-(1H-indol-3-ylmethyl)-3-methyl-4,9-dioxo-7-phenyl-12-oxa-2,5,8-triaza-11-phosphatetradecanoic acid 11-oxide tricyclo<3.3.1.1^3,7>dec-2-yl ester

There total 1 articles about -11-ethoxy-3-(1H-indol-3-ylmethyl)-3-methyl-4,9-dioxo-7-phenyl-12-oxa-2,5,8-triaza-11-phosphatetradecanoic acid 11-oxide tricyclo<3.3.1.1^3,7>dec-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethylphosphonoacetic acid (3095-95-2) + tricyclo<3.3.1.13,7>dec-2-yl *,R*)>-<2-<(2-amino-2-phenylethyl)amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamate (130406-64-3) → -11-ethoxy-3-(1H-indol-3-ylmethyl)-3-methyl-4,9-dioxo-7-phenyl-12-oxa-2,5,8-triaza-11-phosphatetradecanoic acid 11-oxide tricyclo<3.3.1.13,7>dec-2-yl ester (141956-41-4)

Guidance literature:

With 2,3,4,5,6-pentafluorophenol; dicyclohexyl-carbodiimide; Yield given. Multistep reaction; 1.) EtOAc, RT, 3 h, 2.) EtOAc, RT, overnight;

DOI:10.1021/jm00092a007

Reference yield:

-11-ethoxy-3-(1H-indol-3-ylmethyl)-3-methyl-4,9-dioxo-7-phenyl-12-oxa-2,5,8-triaza-11-phosphatetradecanoic acid 11-oxide tricyclo<3.3.1.13,7>dec-2-yl ester (141956-41-4) → -<1-(1H-indol-3-ylmethyl)-1-methyl-2-oxo-2-<<2-phenyl-2-<(phosphonoacetyl)amino>ethyl>amino>ethyl>carbamic acid tricyclo<3.3.1.13,7>dec-2-yl ester (141956-43-6)

Guidance literature:

With trimethylsilyl bromide; water; Yield given. Multistep reaction; 1.) CH₂Cl₂, RT, 36 h, 2.) MeOH, RT, 24 h;

DOI:10.1021/jm00092a007

Reference yield:

-11-ethoxy-3-(1H-indol-3-ylmethyl)-3-methyl-4,9-dioxo-7-phenyl-12-oxa-2,5,8-triaza-11-phosphatetradecanoic acid 11-oxide tricyclo<3.3.1.13,7>dec-2-yl ester (141956-41-4) → -<2-<<2-<<(ethylphosphono)acetyl>amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.13,7>dec-2-yl ester (141956-45-8)

Guidance literature:

With trimethylsilyl bromide; water; Yield given. Multistep reaction; 1.) CH₂Cl₂, RT, 36 h, 2.) MeOH, RT, 24 h;

DOI:10.1021/jm00092a007

upstream raw materials:

diethylphosphonoacetic acid

tricyclo<3.3.1.1^3,7>dec-2-yl *,R^*)>-<2-<(2-amino-2-phenylethyl)amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamate

Downstream raw materials:

-<1-(1H-indol-3-ylmethyl)-1-methyl-2-oxo-2-<<2-phenyl-2-<(phosphonoacetyl)amino>ethyl>amino>ethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester

-<2-<<2-<<(ethylphosphono)acetyl>amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester

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