Boc-Thr(PO2)-OMBzl

Base Information

Chemical Name:Boc-Thr(PO2)-OMBzl
CAS No.:171775-77-2
Molecular Formula:C₃₁H₃₆N₃O₁₃P
Molecular Weight:689.613
Hs Code.:

Synonyms:

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Chemical Property of Boc-Thr(PO2)-OMBzl

Chemical Property:

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Technology Process of Boc-Thr(PO2)-OMBzl

There total 3 articles about Boc-Thr(PO2)-OMBzl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 619-73-8
4-nitrobenzyl chloride

: 171775-77-2
Boc-Thr(PO2)-OMBzl

Guidance literature:: Multi-step reaction with 2 steps

1: 79.9 percent / triethylamine / tetrahydrofuran / 2 h / 0 °C

2: 1.) 1H-tetrazole, 2.) triethylamine, 30percent aq. H₂O₂ / 1.) THF, 1 h, 2.) AcOEt, 0 deg C, 1.5 h

With 1H-tetrazole; dihydrogen peroxide; triethylamine; In tetrahydrofuran;
DOI:10.1246/bcsj.68.2699

Reference yield:

: 2592-18-9
Boc-Thr-OH

: 171775-77-2
Boc-Thr(PO2)-OMBzl

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) aq. Cs₂CO₃, 2.) NaI, Cs₂CO₃ / 1.) MeOH, 2.) DMF, RT, overnight

2: 1.) 1H-tetrazole, 2.) triethylamine, 30percent aq. H₂O₂ / 1.) THF, 1 h, 2.) AcOEt, 0 deg C, 1.5 h

With 1H-tetrazole; dihydrogen peroxide; caesium carbonate; triethylamine; sodium iodide;
DOI:10.1246/bcsj.68.2699

Reference yield:

: (2S,3R)-2-tert-Butoxycarbonylamino-3-hydroxy-butyric acid 4-methoxy-benzyl ester

: 143057-36-7
N,N-diisopropyl-di(4-nitrobenzyl)phosphoramidite

: 171775-77-2
Boc-Thr(PO2)-OMBzl

Guidance literature:: With 1H-tetrazole; dihydrogen peroxide; triethylamine; Multistep reaction; 1.) THF, 1 h, 2.) AcOEt, 0 deg C, 1.5 h;
DOI:10.1246/bcsj.68.2699