diphenylphosphino-2-bis(p-fluorophenyl)phosphinoethanetetracarbonylmolybdenum⁽⁰⁾

Base Information

• Chemical Name: diphenylphosphino-2-bis(p-fluorophenyl)phosphinoethanetetracarbonylmolybdenum⁽⁰⁾
• CAS No.: 106005-84-9
• Molecular Formula: C₃₀H₂₂F₂MoO₄P₂
• Molecular Weight: 642.387

Synonyms:

Chemical Property of diphenylphosphino-2-bis(p-fluorophenyl)phosphinoethanetetracarbonylmolybdenum⁽⁰⁾

Chemical Property:

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Technology Process of diphenylphosphino-2-bis(p-fluorophenyl)phosphinoethanetetracarbonylmolybdenum⁽⁰⁾

There total 1 articles about diphenylphosphino-2-bis(p-fluorophenyl)phosphinoethanetetracarbonylmolybdenum⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-diphenylphosphino-2-bis<(p-fluoro)phsphino>ethane (94940-45-1) + molybdenum hexacarbonyl (13939-06-5,199620-15-0) → diphenylphosphino-2-bis(p-fluorophenyl)phosphinoethanetetracarbonylmolybdenum(0) (106005-84-9)

Guidance literature:

In methyl cyclohexane; under N2 atm., Schlenk tube techniques; reflux of mixt. of Mo(CO)6 and P compd. in methylcyclohexane; removal of solvent in vac.; chromy. (silica, chloroform); recrystn. from chloroform/hexane; elem. anal.;

DOI:10.1016/0022-328X(86)80224-8

Reference yield:

diphenylphosphino-2-bis(p-fluorophenyl)phosphinoethanetetracarbonylmolybdenum(0) (106005-84-9) → diphenylphosphino-2-bis(p-fluorophenyl)phosphinoethanetricarbonylpyridinomolybdenum(0)

Guidance literature:

With pyridine; In not given; under N2 atm., Schlenk tube techniques; refluxing of Mo-complex with anexcess of pyridine in methylcyclohexane for ca 40h; elem. anal.;

DOI:10.1016/0022-328X(86)80224-8

upstream raw materials:

1-diphenylphosphino-2-bis<(p-fluoro)phsphino>ethane

molybdenum hexacarbonyl

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