(+)-1-phenyl-3-diphenylphosphinoyl-1,2,3,6-tetrahydrophosphinine oxide

Base Information

• Chemical Name: (+)-1-phenyl-3-diphenylphosphinoyl-1,2,3,6-tetrahydrophosphinine oxide
• CAS No.: 1235834-98-6
• Molecular Formula: C₂₄H₂₃ClO₂P₂
• Molecular Weight: 440.846
• Mol file: 1235834-98-6.mol

Synonyms:

Chemical Property of (+)-1-phenyl-3-diphenylphosphinoyl-1,2,3,6-tetrahydrophosphinine oxide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (+)-1-phenyl-3-diphenylphosphinoyl-1,2,3,6-tetrahydrophosphinine oxide

There total 1 articles about (+)-1-phenyl-3-diphenylphosphinoyl-1,2,3,6-tetrahydrophosphinine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(-)-3-methyl-4-chloro-1-phenyl-1,2-dihydrophosphinine 1-oxide + Diphenylphosphine oxide (4559-70-0) → (-)-1-phenyl-3-diphenylphosphinoyl-1,2,3,6-tetrahydrophosphinine oxide + (+)-1-phenyl-3-diphenylphosphinoyl-1,2,3,6-tetrahydrophosphinine oxide (1235834-98-6)

Guidance literature:

Diphenylphosphine oxide; With trimethylaluminum; In chloroform; at 0 ℃; for 20h;

(-)-3-methyl-4-chloro-1-phenyl-1,2-dihydrophosphinine 1-oxide; In chloroform; water; at 0 ℃; optical yield given as %ee; diastereoselective reaction;

DOI:10.2174/157017810790796345

upstream raw materials:

Diphenylphosphine oxide