((CH₃)3C₆H₂NCH₂CH₂)2NCH₂CH₂N(⁽¹³⁾CH₃)C₆H₂(CH₃)3Zr(N(CH₃)2)2

Base Information

Chemical Name:((CH₃)3C₆H₂NCH₂CH₂)2NCH₂CH₂N(⁽¹³⁾CH₃)C₆H₂(CH₃)3Zr(N(CH₃)2)2
CAS No.:359911-68-5
Molecular Formula:C₃₈H₆₀N₆Zr
Molecular Weight:693.148
Hs Code.:

((CH<sub>3</sub>)3C<sub>6</sub>H<sub>2</sub>NCH<sub>2</sub>CH<sub>2</sub>)2NCH<sub>2</sub>CH<sub>2</sub>N(<sup>(13)</sup>CH<sub>3</sub>)C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3Zr(N(CH<sub>3</sub>)2)2

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Chemical Property of ((CH₃)3C₆H₂NCH₂CH₂)2NCH₂CH₂N(⁽¹³⁾CH₃)C₆H₂(CH₃)3Zr(N(CH₃)2)2

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Technology Process of ((CH₃)3C₆H₂NCH₂CH₂)2NCH₂CH₂N(⁽¹³⁾CH₃)C₆H₂(CH₃)3Zr(N(CH₃)2)2

There total 2 articles about ((CH₃)3C₆H₂NCH₂CH₂)2NCH₂CH₂N(⁽¹³⁾CH₃)C₆H₂(CH₃)3Zr(N(CH₃)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 219598-45-5
N(CH₂CH₂NH-2,4,6-C₆H₃(CH₃)3)3

: 359911-68-5
((CH₃)3C₆H₂NCH₂CH₂)2NCH₂CH₂N(⁽¹³⁾CH₃)C₆H₂(CH₃)3Zr(N(CH₃)2)2

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: CH₃Li / tetrahydrofuran

With CH₃Li; In tetrahydrofuran; toluene;
DOI:10.1021/om010247k

Reference yield:

: 4227-95-6
[13C]methyl iodide

: 359911-62-9
((CH₃)3C₆H₂NCH₂CH₂)2NCH₂CH₂NHC₆H₂(CH₃)3Zr(N(CH₃)2)2

: 359911-68-5
((CH₃)3C₆H₂NCH₂CH₂)2NCH₂CH₂N(⁽¹³⁾CH₃)C₆H₂(CH₃)3Zr(N(CH₃)2)2

Guidance literature:: With CH₃Li; In tetrahydrofuran; byproducts: CH4; MeLi was added dropwise to a soln. of complex in THF cooled to -20°C, the mixt. was stirred at room temp. for 5 min, an excess of CH3I was added at room temp., the mixt. was left for 35 min (N2);
DOI:10.1021/om010247k

Reference yield:

: 359911-68-5
((CH₃)3C₆H₂NCH₂CH₂)2NCH₂CH₂N(⁽¹³⁾CH₃)C₆H₂(CH₃)3Zr(N(CH₃)2)2

: 15439-85-7
2,6-lutidine hydrochloride

: 359911-69-6
((CH₃)3C₆H₂NCH₂CH₂)2NCH₂CH₂N(⁽¹³⁾CH₃)C₆H₂(CH₃)3ZrCl₂

Guidance literature:: In diethyl ether; byproducts: (CH3)2NH; 2 equiv of lutidinium chloride was added to a soln. of complex in ether at -20°C (N2); ppt. was washed with pentane, dried;
DOI:10.1021/om010247k