15-acetoxyverrucarol

Base Information

Chemical Name:15-acetoxyverrucarol
CAS No.:123301-13-3
Molecular Formula:C₁₇H₂₄O₅
Molecular Weight:308.375
Hs Code.:

Synonyms:

Suppliers and Price of 15-acetoxyverrucarol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 15-acetoxyverrucarol

Chemical Property:

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Technology Process of 15-acetoxyverrucarol

There total 1 articles about 15-acetoxyverrucarol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 108-24-7
acetic anhydride

: 2198-92-7,80514-49-4,123301-12-2
verrucarol

: 2533-38-2,123301-13-3
15-acetoxyverrucarol

: 2198-94-9,123301-16-6
4β,15-diacetoxyverrucarol

Guidance literature:: With pyridine; for 2h; Ambient temperature;
DOI:10.1021/jm00347a018

Reference yield:

: 2533-38-2,123301-13-3
15-acetylverrucarol

: 82521-42-4
C₅₇H₈₆O₉Si₃

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH, HMPA / 1.) THF, 2.) -10 deg C

2: LiOH, H₂O / 1,2-dimethoxy-ethane

3: 1.) NaH, n-Bu₄NI / 1.) THF, 2.) room temp.

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hydroxide; water; tetra-(n-butyl)ammonium iodide; sodium hydride; In 1,2-dimethoxyethane;
DOI:10.1021/jo00138a041

Reference yield:

: 2533-38-2,123301-13-3
C₁₇H₂₄O₅

: 2198-93-8,38757-97-0,74501-22-7
trichodermol

Guidance literature:: Multi-step reaction with 5 steps

1: dimethylformamide

3: methanesulfonyl chloride / dimethylformamide / 70 °C

4: tri-n-butyltin hydride, benzoyl peroxide

With Perbenzoic acid; tri-n-butyl-tin hydride; methanesulfonyl chloride; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)74548-5