Technology Process of C20H28O6S
There total 8 articles about C20H28O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium tert-butylate;
In
ethanol;
for 3h;
Reflux;
DOI:10.1002/chir.20915
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1,4-diaza-bicyclo[2.2.2]octane / ethyl acetate / 4 h / 0 - 20 °C
2: N-ethyl-N,N-diisopropylamine; sodium iodide / acetone / 18 h / 26 - 50 °C
3: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -15 - 0 °C
4: sodium hydroxide / methanol; water / 2.5 h / 50 °C
5: sodium tungstate monohydrate; dihydrogen peroxide; sodium hydrogencarbonate / water; acetone / 18 h
6: potassium tert-butylate / ethanol / 3 h / Reflux
With
1,4-diaza-bicyclo[2.2.2]octane; sodium tungstate monohydrate; potassium tert-butylate; dihydrogen peroxide; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; sodium iodide; sodium hydroxide; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; ethanol; water; ethyl acetate; acetone;
DOI:10.1002/chir.20915
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -15 - 0 °C
2: sodium hydroxide / methanol; water / 2.5 h / 50 °C
3: sodium tungstate monohydrate; dihydrogen peroxide; sodium hydrogencarbonate / water; acetone / 18 h
4: potassium tert-butylate / ethanol / 3 h / Reflux
With
sodium tungstate monohydrate; potassium tert-butylate; dihydrogen peroxide; sodium hydrogencarbonate; sodium hydroxide; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; ethanol; water; acetone;
DOI:10.1002/chir.20915