[Ru2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(MeCN)(Cp)2][SO3CF3]

Base Information

Chemical Name:[Ru2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(MeCN)(Cp)2][SO3CF3]
CAS No.:850088-37-8
Molecular Formula:CF₃O₃S*C₂₄H₂₅N₂O₂Ru₂
Molecular Weight:724.685
Hs Code.:

Synonyms:

Suppliers and Price of [Ru2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(MeCN)(Cp)2][SO3CF3]

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Chemical Property of [Ru2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(MeCN)(Cp)2][SO3CF3]

Chemical Property:

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Technology Process of [Ru2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(MeCN)(Cp)2][SO3CF3]

There total 1 articles about [Ru2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(MeCN)(Cp)2][SO3CF3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: [Ru2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)2(C5H5)2]CF3SO3

: 75-05-8,26809-02-9
acetonitrile

: 850088-37-8,894806-95-2,894806-93-0
[Ru2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(MeCN)(Cp)2][SO3CF3]

Guidance literature:: With Me₃NO; In acetonitrile; (N2); std. Schlenk technique; Me3NO was added to soln. of Ru complex in MeCN; stirred at room temp. for 1 h; solvent removed (vac.); washed (petroleum ether); dissolved in CH2Cl2; filtered through Celite; solvent removed (vac.); filtered; elem. anal.;
DOI:10.1016/j.jorganchem.2006.01.020

Reference yield: 79.0%

: 850088-37-8,894806-95-2,894806-93-0
[Ru2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(MeCN)(Cp)2][SO3CF3]

: 917-61-3
sodium isocyanate

: 850088-38-9
[Ru2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(isocyanato))(Cp)2]

Guidance literature:: In tetrahydrofuran; under N2; NaNCO (excess) added to soln. of Ru complex in THF; heated at reflux temp. for 3 h; solvent removed in vac.; dissolved in CH2Cl2; chromd. (Al2O3, MeCN); elem. anal.;
DOI:10.1016/j.ica.2004.11.033

Reference yield: 75.0%

: sodium azide

: 850088-37-8,894806-95-2,894806-93-0
[Ru2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(MeCN)(Cp)2][SO3CF3]

: 850088-41-4
[Ru2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(azido))(Cp)2]

Guidance literature:: In tetrahydrofuran; under N2; NaN3 (excess) added to soln. of Ru complex in THF; heated at reflux temp. for 3 h; solvent removed in vac.; dissolved in CH2Cl2; chromd. (Al2O3, THF); elem. anal.;
DOI:10.1016/j.ica.2004.11.033