C₁₇H₂₃N₃O₃

Base Information

Chemical Name:C₁₇H₂₃N₃O₃
CAS No.:1301726-00-0
Molecular Formula:C₁₇H₂₃N₃O₃
Molecular Weight:317.388
Hs Code.:

C<sub>17</sub>H<sub>23</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₁₇H₂₃N₃O₃

Chemical Property:

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Technology Process of C₁₇H₂₃N₃O₃

There total 7 articles about C₁₇H₂₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₄O₄

: 1301726-00-0
C₁₇H₂₃N₃O₃

Guidance literature:: C₁₇H₂₄O₄; With diphenyl phosphoryl azide; triphenylphosphine;

With di-isopropyl azodicarboxylate; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.tetlet.2010.11.013

Reference yield:

: C₂₀H₃₈O₃Si

: 1301726-00-0
C₁₇H₂₃N₃O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium osmate(VI) dihydrate; methanesulfonamide; water; potassium carbonate; 4-[(R)-[(2R,4R,5S)-5-ethyl-1-azabicyclo[2.2.2]octan-2-yl]-(6-methoxy-4-quinolinyl)methoxy]-1-[(R)-[(2R,4S,5R)-5-ethyl-1-azabicyclo[2.2.2]octan-2-yl]-(6-methoxy-4-quinolinyl)methoxy]phthalazine; potassium hexacyanoferrate(III) / tert-butyl alcohol / 22 h / 0 - 10 °C

2.1: lithium borohydride; water / tetrahydrofuran

3.1: sodium hydride; 1-[(2,4,6-triisopropylphenyl)sulfonyl]-1H-imidazole / tetrahydrofuran / 0 °C

4.1: tetrahydrofuran / 0 - 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran

6.1: camphor-10-sulfonic acid / dichloromethane / 20 °C

7.1: diphenyl phosphoryl azide; triphenylphosphine

7.2: 20 °C

With potassium osmate(VI) dihydrate; lithium borohydride; methanesulfonamide; diphenyl phosphoryl azide; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; water; sodium hydride; potassium carbonate; 4-[(R)-[(2R,4R,5S)-5-ethyl-1-azabicyclo[2.2.2]octan-2-yl]-(6-methoxy-4-quinolinyl)methoxy]-1-[(R)-[(2R,4S,5R)-5-ethyl-1-azabicyclo[2.2.2]octan-2-yl]-(6-methoxy-4-quinolinyl)methoxy]phthalazine; triphenylphosphine; potassium hexacyanoferrate(III); 1-[(2,4,6-triisopropylphenyl)sulfonyl]-1H-imidazole; In tetrahydrofuran; dichloromethane; tert-butyl alcohol; 1.1: Sharpless dihydroxylation / 3.1: Fraser-Reid epoxidation;
DOI:10.1016/j.tetlet.2010.11.013

Reference yield:

: 1301725-94-9
C₁₈H₃₈O₄Si

: 1301726-00-0
C₁₇H₂₃N₃O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride; 1-[(2,4,6-triisopropylphenyl)sulfonyl]-1H-imidazole / tetrahydrofuran / 0 °C

2.1: tetrahydrofuran / 0 - 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran

4.1: camphor-10-sulfonic acid / dichloromethane / 20 °C

5.1: diphenyl phosphoryl azide; triphenylphosphine

5.2: 20 °C

With diphenyl phosphoryl azide; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hydride; triphenylphosphine; 1-[(2,4,6-triisopropylphenyl)sulfonyl]-1H-imidazole; In tetrahydrofuran; dichloromethane; 1.1: Fraser-Reid epoxidation;
DOI:10.1016/j.tetlet.2010.11.013